GCMS analysis results, sample AE09972, May 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\9972.D Vial : 20 Acq On 7 May 2002 3:11 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 12 2,5-Dihydrophosphole, 3-met.. Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.58 0.35 ug/L 407275 Phenanthranene-dl0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 4 2 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2/40 4 Phenanthrene, 2-methyl- 192 C15H12 002531-84-2 40 Abundance Scan 3319 (22.580 min): 9972.D (-3312) (-) m/z 192.10 100.00% 192

5000 - 40 7 51 66 90 82 96| 120 146 j 1 60 J 22.20 22.40 22.60 22.80 23.00 I [ । । । I | > r I I | t I Ti । i i i i । । | | । | i t I I । | | i | । i I I i । i i । । । । । i I | i i i i । i । । i [ i i'l r । i i i | 'j । I i r । i i i i । । i । i | 4 m/z 191.10 20.56% /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164

5000 99 115 22.20 22.40 22.60 22.80 23.00 47 77 177 m/z 146.10 13.56% 67 125 134 146 TIT] 27 38.57.L —l+ 4HP 1 1 r 1'1 r 1111 | 155 " I'1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 192 ....... 0......... 22.20 22.40 22.60 22.80 23.00 5000 m/z 193.10 13.09%

96 165 i । 29 39 51 63 74 83 j 115 126 139 152 . 176 , i । । । । । । । । । 11 । । > > | v । r । । i'll । । । i‘i । i’ll r I । । II 11 । । i । rri । 11 t i i । i i r i“| i i1 I j ■ i r i i | i’i i i [ i rli j 11 i'll) "i" mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ..................'................. ) Abundance #125849: Anthracene, 9-methyl- I I ' ' I I I ' I I I 1t l’ I I I I r r I I 192 22.20 22.40 22.60 22.80 23.00 m/z96.00 12.58% 5000

_ 96 165 28 39 51 63 74 83 1 105 115 126 139 152 I 176 1 I ] I । | i'| t r । > | li i i । ITi i| । lli |Ti lT| ill I | । i i I | I if'r |'r> 1'1 j i ri’) 1 I । | l r i 1 | ill i | i ill | i i I r TTTI ............. II।1 ......... 1 । I [ । I Tn pn i ! I | i i f k i m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9972.D 050102 .M Tue May 07 15:50:59 2002 Page 16

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