GCMS analysis results for sample AE09333, May 2002

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Laboratory report documenting GCMS analysis of sample AE09333 conducted on May 8, 2002.

NYC-WTC_000044628–000044649

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050202\9333.D Vial: 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 13 Phenanthrene, 9-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.37 ug/L 420958 Phenanthranene- dl 0 22.96 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 53 2 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 50 3 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H130P 1000196-97-545 4 Phenanthrene, 1-methyl- 192 C15H12 000832-69.9 42 Abundance Scan 3319 (22,580 min): 9333.D (-3312) (-) m/z 192.10 "00.00% 192

5000

40 70 82 J6 118 146 160 1 i 1 ' 22.20 22.40 22.60 22.80 23.00 ... A ■ I I . . . ■ 1 1 . . 1 1 .

< । I I I ! | I I . . | > I I I | I ! I I | 'I'l I I | I I l' I | ! ! ! I | THHTTT 1 ... J... TT H— ) I I I I I I I I I I I I I I m/z 191.10 21.28% /z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #81033: Phenanthrene, 9-methyl- 192

5000 __________ _ _______i r. i . i ] i l rq >iii । । । । । । । । r“

22.20 22.40 22.60 22.80 23.00 m/z 146.10 16.44% 96 165

/z-> "i" ‘ ।" i" " i" 29 39 51 63 73 83 i" " i ■" ‘ i l 115 126 139 152 j 176 i >r 111 ■11111111 ■ ■ ■ 11 ■ ■1111'11ri 11'1111' P11' 11′1′1111 rh 1 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 1 11"

Abundance #80862:1,2-Phenylene diisothiocyanate 192 ................ A................... ■ । 11 11 ।11 ‘ ■ ।1 1 1 1 ।1 11 111 22.20 22.40 22.60 22.80 23.00 64 5000 m/z 193.10 14.65%

75 90 134 39 50 '11"1 4 —8.2+4 _ i1?7 i i I 122 ■I1! r ri"1 r'hrrh 148 160 r , 11 | I1 TT Tl/Z-> Abundance 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 #80965: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 192 1 ....... 1......... l 1 ■ ■ ‘ I ■ ' 1 TT' 1 I I [ I I I I I I

164 22.20 22.40 22.60 22.80 23.00 m/ Z 96.10 13.23% 5000 99 115 47 77 177 67 125 146 27 37. 1,57 || , 87, || | 1.... ‘‘11 । ■1" । i । । । । । । r| rt I TTTTTTTtT 71117741125/++, V TT + 1" I'r « | i i i i | i । i i | 1111LI "I 'T-1 j T m/z—> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 22.20 22.40 22.60 22.80 23.00

9333.D 050102.M Mon May 06 13:56:01 2002 Page 17

NYC-WTC_000044645

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