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GCMS analysis results for sample AE09333, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09333 conducted on May 8, 2002.

NYC-WTC_000044628–000044649

Folder label: “GCMS X 4/29/02 A 5/3/02

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NYC 9/11 Public Portal Document Library yearcn Compound Report

Data File C:\MSDCHEM\1\DATA\050202\9333.D Vial: 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.57 ug/L 637806 Phenanthranene-dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 86 2 Anthracene-dlO - 188 C14D10 001719-06-8 86 3 Antipyrine 188 C11H12N2O 000060-80-0 40 4 Pentacyclo[7.3.1.1. (4,12) .0(2,7) .. . 188 C14H20 1000215-61-8 39 Abundance Scan 3409 (23.109 min): 9333.D (-3403) (-) m/z 188.15 To 0.00% 188

5000

----- 80 94 22.80 23.00 23.20 23.40 42 57 66 , 132 146 158 ||| i । i i > i । i i । i । । i । i । l‘i । i । I I ' । ■ I | । p । { I' । । I ■ | I rTIWTTTTDTETTTTTTTHTTTITTTTTTT i i m/z 94.05 16.91% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

..................... ........................... 5000 ■ ' I ■ 1 1 ■} I 1 I ■ I - ' I I > I 1 I 22.80 23.00 23.20 23.40 m/z 80.10 14.51% 80 94 160 30 42 52 66 11 108 118 132 146 | i p 11 i | i ! i i p r i i | t rt r । I l t r p l l t p t l't | Ft1 1111111 |TTTt]TTu I 11 11 [ 11 I I [ 111 111 "I’l 170179 I... n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188 11 1 i 22.80 23.00 23.20 23.40 5000 m/z 189.15 14.43%

RR 80 94 160 |. 17 30 42 52 0 | 108 118 132 । 111111111111111111111111111111111i1 | 1111 । 11111111111111111111111111111111 146 1 17017911 111111111 ’l’l’t iiii

m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79725: Antipyrine ______ / V ______________ 1 1 i 1 1 ' ' 1 1 1 i ■ 1 r ■ i 1 1 ' 1 I 188 22.80 23.00 23.20 23.40 m/z 184.15 10.62% 96 5000 77 56 105 27 39 । , 67 l Jl 115 130 145 159 173 IL i p > i i p i 1 i l l'l l1! TIIl TTtr 1 । > lli ।' । ri i 11 i'P 11111 ri 111111'| 1111111 >'• । i i rrp-r 1 ' 1 1 1 I I I I I I I I I I-1 “I“I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9333.D 050102.M Mon May 06 13:56:01 2002 Page 18

NYC-WTC_000044646

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