GCMS analysis results for sample AE09333, May 2002

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Laboratory report documenting GCMS analysis of sample AE09333 conducted on May 8, 2002.

NYC-WTC_000044628–000044649

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Data File C:\MSDCHEM\1\DATA\050202\9333.D Vial: 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 15 1,2-Benzenedicarboxylic aci... Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

25.09 0.21 ug/L 233541 Phenanthranene- dl 0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, bu... 362 C22H3404 000089-19-0 72 2 1,2-Benzenedicarboxylic acid, bi... 278 C16H2204 000084-69-5 7, 3 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000085-69-8/ _2 4 1,2-Benzenedicarboxylic acid, bu... 334 C20H30O4 000084-7876 72 Abundance Scan 3747 (25.095 min): 9333. D (-3739) (-) m/z 149.00 100.0 0% 149

5000

--- 24.80 25.00 25.20 25.40 । ■ 11, ■ ■ 41 u 11 76 104 H4 I MH ThTILTTITTUm‘um"u—"E—Otpn0um , 223 m/z 41.10 11.49% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66727: 1,2-Benzenedicarboxylic acid, butyl decyl ester 149

5000 24.80 25.00 25.20 25.40 41 m/Z 150.00 9.50% 2 223 15 , 1 58 76 93 121 i । । । । r ।' । । । । i' r । । 11 r । । । । । । r । i । । । । । > । 167 - | 289307 363 I' |'l 'I 1 r |"n I I | l'l I I ] 1 I I I | I । r r [ ' 11 | i I ■ I | i i ■ I ] i I i r | i I ■ ' |” 1 i ।

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66775: 1,2-Benzenedicarboxylic acid, bis(2-methylpropyl)... 149 1 1 1 1 1 1 ' | 1 ' 7 1 1 ' 1 11 1 1 1 24.80 25.00 25.20 25.40 5000 m/z 57.10 6.98%

29 57 00 J / 76 104121 1 167 189205 [ 278 । ri r । । T । 1 " ’r । / > ; > • •'1 | ‘i ■ ' Y 1 । 1 Tr ■ ii 1 11* । 1TT1 । । । ri i i p ■ । । । i < i i । । । ■ i । । 17 । । । i“r। । । n-| । । > > । । i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #66725:1,2-Benzenedicarboxylic acid, butyl 2-ethylhexyl este Tt I ' T 1 1 I' 1 1 1 1 1 ' 1 I ' ' 149 24.80 25.00 25.20 25.40 m/ Z 43.10 6.55%

5000 M ill 41 1 58 76 104121... 2‘0171701711//111100192220—311051 167 r 1111 205223 261279 11" 11 p 1' ‘ I " '11 1*Ti) 1111) 334 i"1 n TTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280300 320 340 360 24.80 25.00 25.20 25.40

9333.D 050102.M Mon May 06 13:56:02 2002 Page 19

NYC-WTC_000044647

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