GCMS analysis results for sample AE03249, March 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02MAR01\03249.D Vial: 4 Acq On : 1 Mar 2002 6:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 13 1,2-Benzenedicarboxylic aci.. Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.08 ug/L 60268 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 47 2 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 47 3 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 47 4 1,2-Benzenedicarboxylic acid, mo... 278 C16H2204 004376-20-9 25 Abundance Scan 2456 (31.099 min): 03249.D (-) m/z 149.00 100.00% 149 .)...

5000 57 70 83 97 167 43 113 226 239 30.80 31.00 31.20 31.40

m/z-> 0! X 40 - 60 80 100 120 140 / 160 1..................... 207 180 200 220 — 240 m/z 167.00 28.55% Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... 149

5000 ■ ■ i ■ ■ ' i ' ■ ■ ' i ' ' 57 167 — 30.80 31.00 31.20 31.40 71 m/z 57.10 25.77% 83 — 113 1 0+ 11 1 1 1 1 । r t । r 1 i" 1 । 1 1 , . । । 1 , > । > IIIIIIIII/* miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #326907:1,2-Benzenedicarboxylic acid, bis(2-ethylhexyl) e... 149 30.80 31.00 31.20 31.40 5000 m/z 83.10 25.69% 57 167 71 A 83 o- 113 . /

m/z-> Of 40 4460..887 80 100 NE,120...... 140 1160m 1 ■ ' । 180 ■ 1 1 1 1 1 1 ITTn* । । । । । 200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 11.1 1 i ‘ 1 149 30.80 31.00 31.20 31.40 m/z 70.00 24.73%

5000 57 167 71 83 — 113 .

m/z—> 0 - 40 60 -9--l 80 100 120 140 160 1*11* 180 200 220 240 ■ ■ i ■ ' ■ ' i ' 30.80 31.00 31.20 31.40 ■ ■ । < 1 1 i ■ ■

33249.D HP022102.M Mon Mar 04 12:33:36 2002 Page 15

NYC-WTC_000006184