DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02090.D Vial: 7 Acq On : 26 Feb 2002 7:45 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 1,2-Benzenedicarboxylic aci... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.13 ug/L 90916 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,2-Benzenedicarboxylic acid, 3-... 211 C8H5NO6 000603-11-2 83 2 Phthalic acid, diisooctyl ester ... 390 C24H3804 001330-91-2 78 3 1,2-Benzenedicarboxylic acid, di... 390 C24H3804 027554-26-3 78 4 1,2-Benzenedicarboxylic acid, bi... 390 C24H3804 000117-81-7 78 Abundance Scan 2456 (31.099 min): 02090.D (-) m/z 149.00 :100.00% 149

5000 167 57 71 P 43 ' ' i ‘ ' i ' ' 1 1 ■ i ■ ‘ — 83 113 30.80 31.00 31.20 31.40 ......... ....... 240 m/z 167.00 0- IIIIIIIII । ■ ■ > ■ । 1 1 1 ■ | > 37.03% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #131213:1,2-Benzenedicarboxylic acid, 3-nitro- (CAS) $$ 3... 149

5000 M.... . 30.80 31.00 31.20 31.40 167 71 m/z57.10 31.15%

m/z-> ........ 183.113 132 0!1 1 I 1 1 1 -1" r 11 1 1 1 1 1 1 1 1 40 60 80 100 120 1 1 I1 1 1 1 1 1 140 160 180 200 220 240 Abundance #326955: Phthalic acid, diisooctyl ester $$ 1,2-Benzenedic... 149 A..A.N 30.80 31.00 31.20 31.40 5000 m/z 71.1.0 23.81% 57 167 71

mfe-> O-—TT — 40 60 80 J. .^ni3... o 100 120 140 160 180 200 ——————————— 220240 Abundance #326921:1,2-Benzenedicarboxylic acid, diisooctyl ester (C... ■ ■ i ' ■ i ' ■ ■ ■ i ' ■ 149 30.80 31.00 31.20 31.40 m/z 70.00 21.79%

5000 57 167 71

O-—T 83 — 113 I |l ' I'11’ ' * 1 * 1, I 1 1 1 1 1 1 I ' I ' 'l . 1 I | I I TI | 1 1 1 1 I 1 1 1 1 I 1 1 ....... 11....... m/z—> 40 60 80 100 120 140 160 180 200 220 240 30.80 31.00 31.20 31.40

02090.D HP022102.M Wed Feb 27 08:35:29 2002 Page 15

NYC-WTC_000004683

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NYC-WTC_000004683Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999