GCMS analysis results for sample AE03249, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03249 conducted on March 15, 2002.

NYC-WTC_000006166–000006185

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03249.D Vial: 4 Acq On : 1 Mar 2002 6:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 12 Tetrapentacontane, 1,54-dib... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 28.50 0.09 ug/L 66111 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetrapentacontane, 1,54-dibromo- 915 C54H108Br2 000000-00-0 59 2 1-Hentetracontanol (CAS) $$ N-HE... 593 C41H840 040710-42-7 47 3 1-Hentetracontanol 593 C41H840 040710-42-7 47 4 1-Decanol, 2-ethyl- 186 C12H260 021078-65-9 43 Abundance Scan 2226 (28.503 min): 03249. D (-) m/z 57.10 100.00% 57

u 97 5000

207 Ma 28.20 28.40 28.60 28.80 0 T’TT 1‘1‘111111111117TTT77-17TTT111111"‘7‘11‘1‘‘"‘0‘77-1‘‘‘‘1‘TT‘.‘T""‘TT m/z 55.05 78.27% n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 Abundance #391162: Tetrapentacontane, 1,54-dibromo- 57

5000 97 MAAMA/W W ■ 1 1 । 1 1 ' । * ■ < । n । । * । ' ■ ■ ■ 28.20 28.40 28.60 28.80 m/z 71.00 75.88% J ..................................... . 0 T-r-fT '11 " ’ i'' ■ ■ । ■1 r 11 ■ r ■' ■ r ■ ■ ■ r ■ ■1111111'' ■11 ■ ■ ■ ■ r 11 11 ‘ ■1 'T'11111111 Tr’l 1 835 m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 Abundance #381315:1-Hentetracontanol (CAS) $$ N-HENTETRACONTANOL-1 57

97 28.20 28.40 28.60 28.80 5000 m/z 97.00 62.89%

194 236 574 0 TI1" m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 Abundance #381314:1-Hentetracontanol 1 r I '1 57 28.20 28.40 28.60 28.80 m/z 43.10 54.56%

kp 97 5000

. 574 0 T-rp- ' ' I 1 ' ' ' I ' ' ' 1 1 1 ' ' 1 « । | i । r . j » i . i । i । I I | I I J I '| I I*! I | ।। "11"1111"111 n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 650 700 750 800 28.20 28.40 28.60 28.80

13249.D HP022102.M Mon Mar 04 12:33:36 2002 Page 14

NYC-WTC_000006183

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GCMS analysis results for sample AE03245, March 2002 · Box DEP Box 12

NYC-WTC_000006085

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03245 conducted on March 15, 2002.

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