GCMS analysis results for sample AE03249, March 2002

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02MAR01\03249.D Vial: 4 . Acq On : 1 Mar 2002 6:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 lH-Purin-6-amine, N-methyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 24.85 0.04 ug/L 35736 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1H-Purin-6-amine, N-methyl- 149 C6H7N5 000443-72-1 7 2 3,6-Dimethyl-triazolo(4,3-b) (1,2... 149 C6H7N5 000000-00-0 7 3 3,6-DIMETHYL-TRIAZOLO[4,3-B]-1,2... 149 C6H7N5 061139-71-7 7 4 4-PYRROLIDINOPYRIDAZINE $$ Pyrid... 149 C8H11N3 069698-08-4 4 Abundance Scan 1902 (24.845 min): 03249. D (-) m/z 149.00 100.00% 149

5000

i ■ ■ ■ ■ । ■ 41 49 57 24.60 24.80 25.00 25.20 oH . .......... Il .1 "I, .0—2020—0020002110101101111.00110100 m/z41.10 10.18% TTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44975:1 H-Purin-6-amine, N-methyl- 149

5000 93 120 1, 1717,7 , 1/ [I, 24.60 24.80 25.00 25.20 m/ Z 150.00 9.67% 36 57 66 134 0} ■ ■. rj , ,' 1 .1 ....... I, .............. i ' 1 1 1 i ' 1 ' ' i ■ ■ 1 1 i ' ■ ' 1 i ' 'I।।11I1111I1' - - n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44984: 3,6-DimethyI-triazolo(4,3-b)(1,2,4)-triazine 149

24.60 24.80 25.00 25.20 5000 81 m/ Z 57.00 7.29%

41 53 121 M 0b miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44967: 3,6-DIMETHYL-TRIAZOLO[4,3-B]-1,2,4-TRIAZINE $$1,2... ' 1 i ■ 1 1’ 1 ' i 1‘ 149 24.60 24.80 25.00 25.20 m/z 43-10 7.06%

5000 81

41 53 121 0b ‘ I’’ ■ i ' ■ ■ ■ i 1 — 11' ■ ■ ■ ।1 ■1 ■ ।1''11'11111111111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 24.60 24.80 25.00 25.20

)3249.D HP022102.M Mon Mar 04 12:33:35 2002 Page 13

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