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GCMS analysis results for sample AE03249, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03249 conducted on March 15, 2002.

NYC-WTC_000006166–000006185

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006181
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03249.D Vial: 4 . Acq On : 1 Mar 2002 6:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.34 ug/L 277695 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Acridine-D9 188 C13D9N 000000-00-0 86 3 Phenanthrene-diO 188 C14D10 001517-22-2 78 4 1,4-Naphthalenedione, 5-hydroxy-.. . 188 C11H8O3 000481-42-5 64 Abundance Scan 1718 (22.768 min): 03249.D (-) m/z 188.10 100.00% 188

5000 ............ / -............................ 94 22.40 22.60 22.80 23.00 41 52 66 80 132 0- | > | ]HLi i i‘| I I i'i । i I I i ।'i । I I | i i । i [ I—r IPmmTT It’ 146 160 | L m/Z 189.10 16.99% m/z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 A 5000 22.40 22.60 22.80 23.00 80 94 m/ z 94.00 16.58%

n/z-> 0- 66 nuntt TTTPTFTTTTTTTTTTTTH— ■ 1111 ■111'111111111 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 —Ll Abundance #85254: Acridine-D9 188 - 22.40 22.60 22.80 23.00 5000 m/ z 184.10 10.88%

93 158

n/z-> 0- '' 11 " ' 11''' I " 1' 11'1 ‘ I " “ 111'1111 " I'' “ I'11' I' " ' I ‘ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 . .... 4k, .................................... ................. Abundance #84499: Phenanthrene-d10 188 22.40 22.60 22.80 23.00 m/z 160.10 8.87%

5000

80 94 160 66 m/z-> 0 mmTTTTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Hl..... ’W... ............ ............ ............................. 22.40 22.60 22.80 23.00

53249.D HP022102.M Mon Mar 04 12:33:35 2002 Page 12

NYC-WTC_000006181

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NYC-WTC_000006181Source: NYC Law Department, mirrored locally

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