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GCMS analysis results for sample AE03252, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03252 conducted on March 15, 2002.

NYC-WTC_000006226–000006245

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006240
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03252.D Vial: 7 . Acq On 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.46 ug/L 358802 Phenanthrene -dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 90 2 Anthracene-D10 188 C14D10 000000-00-0 59 3 Anthracene-diO- 188 C14D10 001719-06-8 53 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 50 Abundance Scan 1718 (22.768 min): 03252.D (-) m/z 188.10 100.00% 188

5000

94 . । . . . . . TP ~ j , . . . ! , . . . । . 158 22.40 22.60 22.80 23.00 44 52 66 80 m/z 0- ........ . ~l~p.Hl....111................ 1110 132. . ........ .... 211 . Pun 94.00 17.17% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 ...IL,....... 22.40 22.60 22.80 23.00 80 94 m/z 189.10 11.79% A m/z-> 66 01 11111111 rri 11111111 40 50 60 70 . ——mPmmmmmmm—T 80 90 100 110 120 130 140 150 160 170 180 190 158 .. l... Abundance #84498: Anthracene-D10 188

22.40 22.60 22.80 23.00 5000 m/z 184.10 9.07% 80 94 66

miz-> 0- 40 m— 80 160 ll mg.. . 11L.. ... । rlll.. 50 60 180 190 70 p p 90 100 110 120 130 140 150 160 170 T’l

Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 m/z 158.05 8.49%

5000

80 94 160 , , 66

n/z-> 0 11111" i1 mm 11111111 40 50 60 70 80 > > 111'' 111'. 111 > > ]' > । ।'' ■' । > 90 100 110 120 130 140 150 160 170 180 190 .... I.... w,... n ................................................... .. 22.40 22.60 22.80 23.00

3252.D HP022102.M Mon Mar 04 12:33:55 2002 Page 11

NYC-WTC_000006240

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NYC-WTC_000006240Source: NYC Law Department, mirrored locally

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