GCMS analysis results for sample AE00615, Feb 2002

NYC 9/11 Public Portal Document

Data File : C : \MSDCHEM\1\5973N\02JAN29\00615 . D Vial : 4 Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.46 ug/L 374724 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 91 2 Anthracene-DlO 188 C14D10 000000-00-0 91 3 Anthracene-dlO- 188 C14D10 001719-06-8 90 4 Phenanthrene-diO 188 C14D10 001517-22-2 72 Abundance Scan 1699 (22.771 min): 00615. D (-) m/z 188.10 100.00% 188

5000

80 94 ... R . ....... 22.40 22.60 22.80 23.00 23 20

m/z-> 30 40 52 64 P 40 | 50 60 70 80 132 158 I FIT ■ 111 > । ■ 111111 •r 1111 > • rP ■ । ’ ... 111111 "l’T 90 100 110 120 130 140 150 160 170 180 190 L m/z 94.10 15.99% Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 189.10 14.79%

m/z-> 30 ......................... 66 40 50 60 70 111111 158 TIIPPP 80 90 100 110 120 130 140 150 160 170 180 190 —l Abundance #84498: Anthracene-D10 188 Measi -pi । M । 22.40 22.60 22.80 23.00 23.20 5000 m/z 80.10 12.25% 80 94 66 160

m/z-> Ir''' i ■ ■111' — PP)PPRTH 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 JU ... — .. — I I > I .... I .

Abundance #84502: Anthracene-d10- 188 22.40 22.60 22.80 23.00 23.20 m/z 184.10 11.98%

5000

— 80 94 66 । । 160 । I m/z—> --- ........... .......... lib...... 1894) 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 । ■1 ‘ ■ । 1 r1 1 1 'i 22.40 22.60 22.80 23.00 23.20 ■ 11 1

00615.D SCAN508.M Wed Jan 30 09:02:21 2002 Page 12

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