GCMS analysis results for sample AE00615, Feb 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN29\00615.D Vial: 4 Acq On : 29 Jan 2002 5:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-Amino-5,5-dimethyl-2-meth. .. Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

29.69 0.05 ug/L 36029 Chrysene-dl2 30.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-Amino-5,5-dimethyl-2-methoxyca. .. 243 C15H17NO2 118089-29-5 5 2 2,6-Bis(1,1-dimethylethyl)-4-cya... 243 C16H21NO 007062-57-9 5 3 3-Phenyl-4-azafluorene 243 C18H13N 000000-00-0 5 4 3 -AMINOBENZO(C)PHENANTHRENE 243 C18H13N 000000-00-0 5 Abundance Scan 2305 (29.690 min): 00615.D (-) m/z 244.10 100.00% 24,4 ....... )

5000 40 84 108 122 1 ■ i 1 ' 29.40 29.60 29.80 30.00 ■ 1 i 1 1 1TT m/z 243.10 74.84% m/z-> 40 60 80 100 120140 160 180 200 220 240 Abundance #177722:4-Amino-5,5-dimethyl-2-methoxycarbonyl-3-phenyl-c... 24.4

5000 ‘ It* ' 1 l 29.40 29.60 29.80 30.00 m/ z 40.00 27.66%

m/z-> 0- ............ 40 60 80 167 184 196 212 .. 100 120 140 160 180 200 220 240 Abundance #177862: 2,6-Bis(1,1-dimethylethyl)-4-cyanomethylenecycloh... 243 201 Tl 29.40 29.60 29.80 30.00 159 188 228 m/z 122.10 27.59% 5000 172 128 214 n/z-> ■ 1 i 1 1 40 ‘ 60 । ■ • ' ■ । ■ 80 100 120 I1' 140 160 180 I 200 220 240 Abundance #177934:3-Phenyl-4-azafluorene 243 29.40 29.60 29.80 30.00 m/z 121.70 25.96%

5000

..... 63^ 77 121 ................... . ... ■ I’l’l " T ' ■ i ■ ‘ ' i 1 1 m/z--> 40 60 80 100 120 140 160 180 200 220 240 29.40 29.60 29.80 30.00

00615.D SCAN508.M Wed Jan 30 09:02:21 2002 Page 13

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