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GCMS analysis results for sample AE00108, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.

NYC-WTC_000050754–000050773

Folder label: “GCMS X 1/4/02 A 1/25/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN25\00108.D Vial: 6 . Acq On : 25 Jan 2002 2:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T 22.28 0.14 ug/L 105083 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 3 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 50 4 2-Imidazolidinone, 1-methoxy-3-p... 192 C10H12N2O2 052420-43-6 47 Abundance Scan 1656 (22.280 min): 00108. D (-) m/z 192.10 100.00% 192

5000 ------- 70 82 118 96146 160 II 22.00 22.20 22.40 22.60 44 111111 ■ i ‘ TTTrr' -HH TIPHTPTTT ----- TT" m/Z 191.00 15.58% m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 H I " oMI* I i |i ri i I 22.00 22.20 22.40 22.60 146 175 m/z 193.10 15.10%

n/z-> TTp-rTTp-rTTp-TTTpTTTTTTTTpTTrp-T 40 50 I ” '1I ''"I" " I " 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ r ■ ■ ■ i' " ■ i' । ■ i <" ■ i' u Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 TRBnngm ..... ..i 22.00 22.20 22.40 22.60 5000 m/z 146.10 14.41%

96 mm 139 152 165 176 UIB—0"T—UOITUTTTTTTTTrT TITT /z-> Abundance 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103420:2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 ............... / .. 22.00 22.20 22.40 22.GQ + m/z96.10 13.13%

5000

■ * i ■" ‘ i' j। ■I 9 138 T < f ■ i' ■ l 11 I IT"1 ■ > 111 i 11 n > i rrl’l m i । 11 1111 I i 11 i i i i । rri i j1 । 1. 1. 1. ' 1 I /' TTTemrrgT m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30108.D SCAN508.M Mon Jan 28 09:50:00 2002 Page 14

NYC-WTC_000050771

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NYC-WTC_000050771Source: NYC Law Department, mirrored locally

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