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GCMS analysis results for sample AE03185, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006083
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03185.D Vial: 5 • Acq On : 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 77698 Phenanthrene-dl0 22.63 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 59 3 Phenanthrene, 1-methyl- (CAS) $$... 192 C15H12 000832-69-9 59 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1675 (22.283 min): 03185.D (-) m/z 192.00 100.00% 192

5000

96 ..... /I.... A,, n/z-> Abundance 0 44 ' ■ i ■ ■ ■ > । ■1 ■ ■ i ■ ■ > ■ । 70 82 ■ i ■ |. 11 i.. ]. 120 111111111 > 1111

30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... .11,150..i TT" 22.00 22.20 22.40 22.60 m/z 191.00 N 17.74%

192

108 5000 22.00 22.20 22.40 22.60 146 175 m/ z 96.00 15.73%

0- 11111' i " ■11 ■ +I—TT ‘I‘ n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102434:1,5-Naphthalenedithiole 192 1 ' 1 1 ' ' 1 1 1 22.00 22.20 22.40 22.60 5000 m/z 146.10 15.05% 115 128 159 A 147 33 ...... 01 TITh 111" 11" " i " 111" " i " " r '11102 1 " r ' " i" TIII ,1 111" I11" I " " 11'fl l11 miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103927: Phenanthrene, 1-methyl- (CAS) $$ 1-Methylphenanth... 192 .1 .. Av 22.00 22.20 22.40 22.60 m/z 193.00 13.07%

5000

82 94

m/z—> 0 a 139 152 165 176 > ' | " I " ' 1 | " "I " 1 । |1 ' । 11 i’rn fn ttpunni 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । 22.00 22.20 22.40 22.60

33185.D HP022102.M Mon Mar 04 12:33:00 2002 Page 15

NYC-WTC_000006083

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NYC-WTC_000006083Source: NYC Law Department, mirrored locally

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