GCMS analysis results for sample AE03185, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document LIbrary searen Compound Report

Data File : C:\MSDCHEM\1\5973N\02MAR01\03185.D Vial: 5 Acq On : 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 URACIL DIMETHYL Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.03 ug/L 20020 Acenaphthene-dl0 18.33 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 URACIL DIMETHYL 140 C6H8N202 000000-00-0 7 2 2,4(1H,3H)-Pyrimidinedione, 1,3-. . . 140 C6H8N202 000874-14-6 7 3 2,4(1H,3H)-Pyrimidinedione, 1,3- .. . 140 C6H8N202 000874-14-6 7 4 2,4(1H,3H)-Pyrimidinedione, 3,6-... 140 C6H8N202 019674-60-3 7 Abundance Scan 1167 (16.548 min): 03185.D (-) m/z 140.10 100.00% 140

5000 172 43 56 71 122 ... I.. I, 0- 1111 ' i111111111111 111111111 ■ i ■ ■ ‘ ‘ i * ■ ■ ■ i ‘ I’’ 1 ■ 11 ■ 11 1 '1 I 11 16.20 16.40 16.60 16.80 m/z 172.10 31.13% m/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #35156: URACIL DIMETHYL A 140

55 5000 83 16.20 16.40 1 6.60 16.80 m/z 138.10 20.53% 42 il , 96 ID 0------ ■ 1 ■ J । ■ 1 1 1 1 |T| i ' 1 ' 1 1 1 " 1 1 1 1 1 1 1 1 ' | 111’11111111111111111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35145: 2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- 42 140

55 16.20 16.40 16.60 16.80 83 5000 m/z 136.10 19.55%

iz-> oV 20 H -H TIF 96 111 | " । ■ ■1 ■ i ■1 ■11'11" ।11 ’1111 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 ' " ■ i ‘' i 11'' i11' ' i'

Abundance #35146: 2,4(1 H,3H)-Pyrimidinedione, 1,3-dimethyl- $$ Uraci... 140 16.20 16.40 16.60 16.80 m/z 122.10 17.48% 55 5000 83

m/z—> 0-TWTTTTTTTHTTTT 20 30 40 50 60 70 —M M 80 90 100 110 120 130 140 150 160 170 ‘ 1 1 1 1 1 ■ I 1 1 16.20 16.40 16.60 16.80

3185.D HP022102.M Mon Mar 04 12:33:00 2002 Page 14

NYC-WTC_000006082

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