GCMS results for sample AE00700, Feb 13 2002

NYC 9/11 Public Portal Document LlDrary searen compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\00700.D Vial: 7 Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 9 Uracil, 5-ethyl- $$ 2,4(1H,... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.04 ug/L 19514 Naphthalene-d8 13.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N202 004212-49-1 64 No 2 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 56 Gos 3 Pyridine, 4-nitro-, 1-oxide (CAS... 140 C5H4N2O3 001124-33-0 50 pwcW 4 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 Abundance Scan 876 (13.375 min): 00700.D (-) m/z 140.10 100.00% 140

5000

1 ■ i ■ ■ ' ■ i ■ TT 70 96 13.00 13.20 13.40 13.60 13.80

n/z-> 0 ..... 30 44........ 40 50 60 1.170....8044.11.,. 90 100 110 120 130 140 m/ Z 96.00 11.95% Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 1-0 125 82 5000 ■ i > > > ■ । ■ IT 13.00 13.20 13.40 13.60 13.80 54 m/ z 94.10 11.23% 68 96 — 111 0 - ■ I ■ .H ■ I ■ I Tl/Z--> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089: 2-Methoxy-3-hydrazinyl-pyrazine 140 IT 13.00 13.20 13.40 13.60 13.80 5000 42 m/ Z 70.10 10.20% 54 68 80 95 108 121 of ' ' i 1 ■ ■ i ' ■ TTT ... ........ II, I I —1 ‘IT n/z-> 30 40 50 60 80 70 90 100 110 120 130 140 Abundance #35067: Pyridine, 4-nitro-, 1-oxide (CAS) $$ p-Nitropyridi... TT TF 1.0 13.00 13.20 13.40 13.60 13.80 m/z 141.10 9.47%

5000 39 110 51 45 63 84 94

n/z-> 0 PP 30 ponomp... . 40 50 60 1111111111 "n 1'1 111 1 70 80 90 100 110 120 130 140 TF 13.00 13.20 13.40 13.60 13.80 IT

)0700.D SCAN508.M Mon Feb 04 08:40:52 2002 Page 11

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