DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB26\02016.D Vial: 4 Acq On : 26 Feb 2002 12:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 9 Uracil, 5-ethyl- $$ 2,4(1H,... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 13.38 0.07 ug/L 54056 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Uracil, 5-ethyl- $$ 2,4(1H,3H)-P... 140 C6H8N202 004212-49-1 40 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 3 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 38 4 2-Hydroxy-5-nitropyridine $$ 5-N... 140 C5H4N2O3 005418-51-9 33 Abundance Scan 886 (13.376 min): 02016.D (-) m/z 140.00 100.00% 140 fl 5000

43 59 81 ll I 108 121 m 13.00 13.20 13.40 13.60 13.80

m/z-> Ob 30 —40 L 50 1 । 1 ‘ ----- ■ i ' 60I 70 80 —H 90 100 110 120 130 140 T7I m/ Z 70.00 15.80% Abundance #35153: Uracil, 5-ethyl- $$ 2,4(1 H,3H)-Pyrimidinedione, 5-... 140 125 82 5000- "IT 1 1 ' 1 1 1 1 1 13.00 13.20 13.40 13.60 13.80 54 m/z 59.00 15.37% 68 96 | 111 m/z-> oh 30 1 ' i ' 1 1 ' i ' 40 50 .....l 60 |70.....80 TTi . I'. । . . . . pi . . . । . . I । । । ' 90 100 110 120 130 140 T’i

Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 ■ । > > 1 ' । ■ * 1 ■ i ■ ■ • ■ i ■ 13.00 13.20 13,40 13.60 13.80 5000 m/z 94.00 14.93% 44 71 123 86 96 112 oh■. . . 11 . ---------- l 1Bl miz-> 301 40 50 60 70 80 90 100 110 120 130 140 Abundance #35089:2-Methoxy-3-hydrazinyl-pyrazine TI 1 1 1 ■ ■ ■ i' ■ ■ 1 i ■ 140 13.00 13,20 13.40 13.60 13.80 m/ Z 96.10 11.94%

5000 42 54 68 —80 ............ 95 108 121 Of-.-. ,■ , 1 ' I ' .1......... 1. .I TTI mtz.-> 30 40 50 60 70 80 90 100 110 120 130 140 ■ i 1 ■ 1 1 i 1 1 1 1 1 1 1 1 1 1 1 13.00 13.20 13.40 13.60 13.80

02016.D HP022102.M Wed Feb 27 08:34:33 2002 Page 11

NYC-WTC_000004539

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999