GCMS results for sample AE00700, Feb 13 2002

NYC 9/11 Public Portal Document -1

Data File : C:\MSDCHEM\l\5973N\02FEB01\00700.D Vial: 7 . Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : February 1, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4H-Pyran-4-one, 2-ethyl-3-h... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 16.55 0.05 ug/L 32345 Acenaphthene-diO 18.34 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4H-Pyran-4-one, 2-ethyl-3-hydrox. .. 140 C7H803 004940-11-8 7 2 3-Hydroxy-2,2-dimethylhexyl este... 216 C12H24O3 000000-00-0 7 3 6-amino-2-(methylamino)-4(3H)-py... 140 C5H8N40 089181-81-7 5 4 2-Dimethylamino-4,5-dimethyl-oxa... 140 C7H12N20 000000-00-0 5 Abundance Scan 1154 (16.549 min): 00700.D (-) m/z 140.20 100.00% 140

56 71 5000 43 89 122 172 I TT 16.20 16.40 16.60 16.80 0 111'1' i' - ■ i ■»■ • i • I ‘' 1 1 I ' ' '' I ’ 1 ' ' I'''' I l -n-p-m-p- ‘ 1 m/ z 56.10 50.33% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35348:4H-Pyran-4-one, 2-ethyl-3-hydroxy- (CAS) $$ Ethyl... 140

5000 43 71 J.... lb........ 97 16.20 16.40 16.60 16.80 55 125 m/ Z 71.10 46.48% 01■ i •' > ■ i • • • ■ । • i > > ■ ■ i ■ ■ ■ • i • • • ■ i > I ' ' ’ ’ I 1 1 1 ' I' ’'' I ''' * I I" " I" 111 r Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #138515: 3-Hydroxy-2.2-dimethylhexyl ester of butanoic acid 55 71 43 89 16.20 16.40 16.60 16.80 5000 m/z 43.10 28.87% 27

01' I'' " I'''' I’’ ‘ I’’ ‘1‘1111‘17*1‘711111110111109"7-T/T0-111"1+"""-1‘1*1111111"trT33 ■n/z-> Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #35082:6-amino-2-(methylamino)-4(3H)-pyrimidinone 140 170 1 TT 16.20 16.40 16.60 16.80 TT

m/z 172.30 28.64% | 5000 57 111 43 85 95 67 01. ।।। • ..... 1.......... I ■ i ■ • ■ ■ i'1 ■ ■ i'' ■ ’ i ■ I ■ ■ ■ ■ i ■ ■ ■ ■ i11 ■ ■ i ■' ■ ■ i ■ ■ ■ ■ i' IT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

00700.D SCAN508.M Mon Feb 04 08:40:52 2002 Page 12

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