GCMS results for sample AE00700, Feb 13 2002

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GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.

NYC-WTC_000051806–000051824

Folder label: “GCMS X 1/10/02 A 1/16/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\00700.D Vial: 7 • Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise 2002 : February 1, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 89349 Phenanthrene-d10 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 3 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 4 1,5-Naphthalenedithiole 192 C10H8S2 000000-00-0 45 Abundance Scan 1656 (22.280 min): 00700.D (-) m/z 192.10 100.00% 192 ft 5000

49 70 82 96 146 160 .....y.... . 22.00 22.20 22.40 22.60 OT IHr - m/z 96.10 17.31% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 T-r-r-r — 22.00 22.20 22.40 22.60 146 175 m/z 191.10 14.12%

0T ' i " " i ■' " I ■■1' i1 l ' ' ' '“I i ■ ■ ■ ■ i ■ •11111111 ■ i ■ ■'' i ■' ■' r BuunT ‘ I‘* m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/Z 146.10 14.06%

96 164 | 138 1.............Il 0 i ■ ■'' i1'' ■ i'1 ■ ■ i ■ ‘ ■ ■ r ■' ■ i ■' ।' i ■' ■11 ■ ■1' i'1111111 h 11111111111 1' I'''‘I'''' 111TTtm’ miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine A 1 ■ i ■ ■ I ' ' d 1:2 22.00 22.20 22.40 22.60 77 151 m/z 193.10 13.42% 130 93 104 5000 119

177 0 i ■' ■ ■ i ■ ■' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ r '' ■ i '' i ■ TTTT T’E ‘ IT TTTTTTIWTTTWTTTTTTTT ... tt Wz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

0700.D SCAN508.M Mon Feb 04 08:40:52 2002 Page 13

NYC-WTC_000051822

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NYC-WTC_000051822Source: NYC Law Department, mirrored locally

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