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← Document results/DEP Box 28/GCMS X 1/9/02 A 1/29/02
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GCMS blank analysis for sample AE00555, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE00555 conducted between January 29 and February 1, 2002.

NYC-WTC_000051512–000051530

Folder label: “GCMS X 1/9/02 A 1/29/02

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Scanned page image, NYC-WTC_000051526
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NYC 9/11 Public Portal Document

Library Search Compound Report ■ Data File : C:\MSDCHEM\1\5973N\02JAN29\0109B.D Vial: 1 Acq On : 29 Jan 2002 10:31 am Operator: Sample : lab blank 1/9 Inst : Instrumen Mise : January 29, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 89849 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm • CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 46 Abundance Scan 1656 (22.280 min): 0109B.D (-) m/z 192.10 100.00% 192

5000

82 96 146 160 44 22.00 22.20 22.40 22.60

/z—> 42 66 - 118 ' I'' ’' I *''' I'''' 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 L 11’ m/z 96.00 19.82% Abundance #102588: 4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.10 15.90%

H 11" ' I'1 " i " ■ ■ i ■ ■ " i " " i " ■ ■ i ■ " ' i " r ■ ■' i ■ ■ " i " " i ■ ■ ' r ■" i' " ' i1 '"I....... TTh m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 193.10 15.65% A 96 164 | 138 - " i " ■ ■ r ■ " i1" 11" ■' r " 11" ' ■ r ■'11" '' r ■ " i " " i" • । r " ' r " ■ i' 1’1’1 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 I I’’’ ' 1 i ' 1 22.00 22.20 22.40 22.60 m/z 146.10 14.47%

5000 82

54 110 30 94 — mmmmm HP 160 " r " ' i'11111 " 11"111' " 111" 111 -rrp-> 0 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

109B.D SCAN508.M Wed Jan 30 09:02:34 2002 Page 12

NYC-WTC_000051526

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NYC-WTC_000051526Source: NYC Law Department, mirrored locally

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