DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02382.D Vial: 3 Acq On : 27 Feb 2002 12:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L *********************** * * * * ****************************************** Peak Number 9 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.12 ug/L 81815 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 3 Bitoscanate 192 C8H4N2S2 004044-65-9 59 4 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 58 Abundance Scan 1675 (22.283 min): 02382.D (-) m/z 192.00 100.00% 192

5000

96 1. ha 42 66 82 146 160 , 22.00 22.20 22.40 22.60 rn/z-> 0- 11' i1' " i11" i11111' । 4 118 11'1111 " " I " --- 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/ z 96.00 17.55% Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

5000 108 .22.00 ....... H,,,.,, 22.20 22.40 22.60 146 175 m/z 191.00 15.60%

m/z-> 0 11111110‘1"‘1011111101111011111111T i ■ ■ ■ ■ i ■ ■ ■ ■ 11 ■ ■ ■ 11 ■ 1110111111111 1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 11 1 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192 - 22.00 22.20 22.40 22.60 5000 m/z 193.00 14.87%

96 164

mfe-> 0 “ i' " 11' ''11 " " I ‘1 " 11111111 40 50 60 70 80 138 111111111ITI 1111111111111111111 H 90 100 110 120 130 140 150 160 170 180 190 200 1' i"

Abundance #102102: Bitoscanate 192 22.00 22.20 22.40 22.60 m/z 146.10 14.00% 5000 134 160

m/z-> 0 .. 49... 64.76... 1102........ . 90 " i " " i11 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 176 ■ i > ■1 ■ i ■ ■ ■ ■ i .. A. . 22.00 22.20 22.40 22.60

32382.D HP022102.M Thu Feb 28 08:46:49 2002 Page 11

NYC-WTC_000004980

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NYC-WTC_000004980Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999