DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02382.D Vial: 3 Acq On : 27 Feb 2002 12:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Hydrazinecarboxamide, N,N-d... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 20.44 0.05 ug/L 35172 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrazinecarboxamide, N,N-diphen... 227 C13H13N3O 000603-51-0 74 2 Diphenylamine 169 C12H11N 000122-39-4 72 3 Benzenamine, N-phenyl- (CAS) $$ ... 169 C12H11N 000122-39-4 72 4 9,9-dideuterio-4-azafluorene 169 C12H7D2N 000000-00-0 64 Abundance Scan 1512 (20.443 min): 02382.D (-) m/z 169.00 100.00% 169 A

5000 77 84 51 44 I 20.20 20.40 20.60 20.80

m/z-> 0+ a 40 50 60 70 80 ]' ।1 ■'11'11' i ■' ■ ■ i ■ ■ ‘ ■ i ■ ■ ■ ■ ।'1' ■ । 90 100 110 120 130 140 150 160 170 ■1 ■ ।1 ■ 13.1 m/z 168.00 65.20% Abundance #155417: Hydrazinecarboxamide, N,N-diphenyl- $$ Semicarbaz... 169

5000 51 20.20 20.40 20.60 20.80 65 77 84 m/z 167.10 37.48%

m/z-> O+ mg I 1 । 114 ' I5 141 ill i ■ ‘ | ■ ■ < ■ |

40 50 60 70 80 90 100 110 120 130 140 150 160 170 । | । ' l 1 ■ ■ > I ' - ' ' | । I I I | I ! I I | I I I l | > T’T

Abundance #72283: Diphenylamine 169

20.20 20.40 20.60 20.80 5000 m/z 77.00 22.85% 51 77 84 65 D4 141 154 | | 01 1’/’’’71’441711:’11’’’I’ ■ ■ ।111' i1111111111111111111 r 11111111111' 11 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #72280: Benzenamine, N-phenyl- (CAS) $$ DFA $$ DPA $$ DBA... 169 20.20 20.40 20.60 20.80 m/z 84.00 21.74%

5000 / 51 66 77 84 m/z-> 0 p 40 50 60 70 141 154 ' ' i ' ' '' i ' 1 1 1 i ' ' ' ' i ' ' ' ' i 1 1 ' ' Iri i । । I । । । । । 80 90 100 110 120 130 140 150 160 170 1t[ ■ ' i 11 1 1 1 1 20.20 20.40 20.60 20.80 1 ' l ' '

)2382.D HP022102.M Thu Feb 28 08:46:48 2002 Page 10

NYC-WTC_000004979

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NYC-WTC_000004979Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999