GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 1,2-DIPHENYLHYDRAZINE Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 20.46 0.07 ug/L 71635 Acenaphthene-dl0 18.34 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,2-DIPHENYLHYDRAZINE 182 C12H10N2 000000-00-0 78 2 Diazene, diphenyl-, (E)- $$ Azob... 182 C12H10N2 017082-12-1 72 3 Azobenzene $$ Diazene, diphenyl-... 182 C12H10N2 000103-33-3 64 4 1-Triazene, 3,3-dimethyl-1-pheny... 149 C8H11N3 007227-91-0 39 Abundance Scan 1497 (20,465 min): 0201 B.D (-) m/z 77.10 100.00% 77

5000 51 105 152 169 182 A 20.20 20.40 20.60 20.80 ‘ 1 i ‘ ■

0- 11 ■ ■ ■11 ■1111 ■ -rp-n-rp-r ppmmmmm T-rp- m/z 182.10 30.10% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #90112:1,2-DIPHENYLHYDRAZINE 77

................. ,......................... 5000 20.20 20.40 20.60 20.80 51 105 m/z 105.00 182 22.92% 152

miz-> 39 63 011111" 111 "'l " " 1111 'i''i "I 20 30 40 4--TmTTTP ’ 1’ 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ’ Abundance #90092: Diazene, diphenyl-, (E)- $$ Azobenzene, (E)- $$ tr... 77 .. ...7., 20.20 20.40 20.60 20.80 5000 m/z 51.00 21.50% 182 51 27 38 64 , 0-TmPPPWNITTTTTTT " I " " I " " I 105' l115 '' " I ‘ 152 ‘ l " " I' ‘ " I11 ‘' i'' ‘' 11''' i TIIT niz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #90086: Azobenzene $$ Diazene, diphenyl- $$ Azobenzide $$ ... 77 20.20 20.40 20.60 20.80 m/z 169.20 8.24% 5000 51 182 105 । 63 | 115 128 152

/z—> 0-7 1111111111 ■ " I1" " i''I' ■ i "

20 30 40 50 60 70 480— 90 100 110 120 130 140 150 160 170 180 11" " I " 1 ‘ i i" 11111" 11"11' '' I ‘ 'I111।I TT-p — 20.40 20.60 20.80 A--20.20 1 ' ' ' I 1 ' 1 ' 1 1 '

0201B.D SCAN508.M Thu Feb 21 10:18:58 2002 Page 11

NYC-WTC_000004794

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