GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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• Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ************* * * ****************************************************** Peak Number 10 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.17 ug/L 189929 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 64 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 Anthracene, 9-methyl- 192 C15H12 000779-02-2 53 4 9H-Fluorene, 9-ethylidene- (CAS) 192 C15H12 007151-64-6 45 Abundance Scan 1656 (22.280 min): 0201 B.D (-) m/z 192.10 100.00% 1912

5000

82 96 ........... A 22.00 22.20 22.40 22.60 42 52 70 0 '"I........... I' ' | I ■ H ■ | H 118 146 160 TT 1 ! ' > > 1 | 1 n | 1 ' 1 r I i | | ri I i | i । il j' ArTyn II m/z 96.10 15.86% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 n... /I 22.00 22.20 22.40 22.60 96 164 m/z 191.10 14.07% 138 0 ti | > । i rp-i i । । i ! i i-[i i i i । i i-m । i ! I i । i i i । | i i । । | । । i i | > । . J । . . . > ( rn . I ‘ tTansyaasm T-p-l n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 A JHiB 22.00 22.20 22.40 22.60 5000 m/z 193.10 13.20%

■ । . .-I j I 96 165

n/z-> O' 11. ।. 884— 1111’111112 TT 111111 if 111111 i ""i'"'i1'14 139 152 ' 176 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103920: Anthracene, 9-methyl- 192 22.00 22.20 22.40 22.60 m/z 146.10 13.17%

5000

m-s 40 50 60 70 80 %6 ■i 111 11 |->-i 111111 'T'' " । 152 165 176 „ •1 • ।' " । । 11'' '' l'l'' ' i''' 1 • ।

90 100 110 120 130 140 150 160 170 180 190 200 111 ............ A 22.00 22.20 22.40 22.60

0201B.D SCAN508.M Thu Feb 21 10:18:58 2002 Page 12

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