DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB01\31505.D Vial: 6 Acq On : 1 Feb 2002 6:53 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 87527 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole ... 192 C13H8N2 057102-93-9 64 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 31505.D (-) m/z 192.10 100.00% 192

5000

96 82 146 160 22.00 22.20 22.40 22.60 .100119 .7 66 118 01 . l.. I ■ | i ■ I I 1 । 1 1 1 1 ■ i ■ • ■ ■ । > I ।. . 1 ■ i' 1 1 ' i ' 2 m/z 96.10 17.27% /z-> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424: 3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 193.10 14.96% 138 0 ‘I11........1p - l-p-l tt/z—> 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192 ................... .... ................. !

22.00 22.20 22.40 22.60 5000 m/z 146.10 14.62%

96 164 138 0-1PmmLPPTTI - ...I.... T-p-1 mlz-> Abundance 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 A 22.00 22.20 22.40 22.60 m/z 191.00 12.18% 5000

96 165

m/z-> Q. T1———010dt1———uOuunuo0nuT 60 70 80 88 90 II 139 100 110 120 130 140 150 160 170 180 190 200 152 L ' I "176। ' । r ’t 1 22.00 22.20 22.40 22.60

31505.D SCAN508.M Mon Feb 04 10:14:22 2002 Page 12

NYC-WTC_000004143

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NYC-WTC_000004143Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999