DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000003981–000004147

Folder label: “GCMS X 1/29/02 A 2/1/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB01\31505 .D Vial: 6 Acq On : 1 Feb 2002 6:53 pm Operator: Sample : 508 scan fb Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.42 ug/L 290243 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 86 2 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 000000-00-0 50 3 Antipyrine $$ 3H-Pyrazol-3-one, ... 188 C11H12N2O 000060-80-0 50 4 Acridine-D9 188 C13D9N 000000-00-0 50 Abundance Scan 1699 (22.771 min): 31505.D (-) m/z 188.20 100.00% 188

5000

80 94 22.40 22.60 22.80 23.00 23.20

miz-> Of 40 —4454. --HH 50 66 146 156. —I*) 70 80 90 100 110 120 130 140 150 160 170 180 190 60 T^ m/z 94.10 17.49%

Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 23.20 80 94 m/z 184.10 16.95% 66 O+ 011 I 158 I I 1 ' 1 1 1 I । 1 1 I " " I 1 MITT1 > > | r I I V | I I i ! | > I H-[ [ I > I | I < 1 ' | i ‘I’lp >111 mlz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #98580: Pentacyclo[7.3.1 .1 .(4,12).0(2,7).0(6,11)]tetradeca... 188

22.40 22,60 22.80 23.00 23.20 5000 79 m/ z 80.10 16.52% 67 93 131 117 159 |

m/z- > 01 1 1111'11'1111' 11' I'' 40 50 ----- 60 70 80 90 100 110 120 130 140 150 160 170 180 190 „....... I — Abundance #97845: Antipyrine $$ 3H-PyrazoI-3-one, 1,2-dihydro-1,5-di... ■ i ■ 1 188 22.40 22.60 22.80 23.00 23.20 96 m/z 189.10 11.92%

5000 77 56 105 | 146 159 173 0 1' i'111 r ' 111 " 1 11 " ' 111l TTUTTTTTTTTTTTTTTTTTTTTETTTTTTTTTTT II’r JU ............ ........................................ m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

31505.D SCAN508.M Mon Feb 04 10:14:22 2002 Page 13

NYC-WTC_000004144

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999