GCMS analysis results for sample AE00839, Jan 2002

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Laboratory report for sample AE00839 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.

NYC-WTC_000050421–000050431

Folder label: “GCMS X 1/3/02 A 1/22 - 1/23/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00839.D Vial: 8 Acq On : 23 Jan 2002 8:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 74081 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 72 2 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 72 3 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00839.D (-) m/z 192.10 100.00% 19/2

5000 ........................ .............. ..

l1_l 96 82 22.00 22.20 22.40 22.60 0- mH 49 70 —+ ■ ■ l ■1 m/z 96.00 16.53% niz—> 40 50 60 70 80 90 100 110 120 130 140 150 160' 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

5000 22.00 22.20 22.40 22.60 96 164 m/z 193.10 15.81% 138 oV ■ i • ■ ■ ■ l ■ ’1’41’1’14/114 —IPPPmPTTPTTT iz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l .........ill.. -rpn

Abundance . #103420: 2-CYANOCARBAZOLE $$ 9H-Carbazole-2-carbonitrile (CAS 192

22.00 22.20 2240 22.60 5000 m/z 146.10 14.65%

96 164 . 138 ....... ............. i 0 TMTPTTT r> 111 rn 1111111 n 11’* 111 ■1 miz—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... .............. A........... ) Ct ’***}s10*4’I4 p 192 22.00 22.20 22.40 22.60 m/z 191.00 14.18% 108 5000

146 175

n/z—> 0- 40 50 60 70 80 I ■ ■ ‘ ■ i11 ■ • i ■ ■ “ i ■ ■ TTtt’1’’111" HP TTIni 90 100 110 120 130 140 150 160 170 180 190 200 ...... II....A, 22.00 22.20 22.40 22.60

00839.D SCAN508.M Thu Jan 24 09:57:28 2002 Page 5

NYC-WTC_000050429

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