GCMS analysis results for sample AE00839, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN23\00839.D Vial: 8 Acq On : 23 Jan 2002 8:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 Acetamide (CAS) $$ Ethanami... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 9.85 0.13 ug/L 43149 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetamide (CAS) $$ Ethanamide $$... 59 C2H5NO 000060-35-5 4 2 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4 3 3-Pentanol, 2-methyl- (CAS) $$ 2... 102 C6H140 000565-67-3 4 4 Guanidine $$ Aminoformamidine $$... 59 CH5N3 000113-00-8 3 Abundance Scan 567 (9.847 min): 00839.D (-) m/ z 59.10 100.00%

M 59

5000

41 45 73 84 9.60 9.80 10.00 10.20 O+ ...................... II1 49 ‘I*4**I*-‘4I*‘‘‘I*‘*7‘‘-*{** ■11 ■ ■' ■ । ■ - am m/z 45.10 13.96% iUz~> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 9C Abundance #641: Acetamide (CAS) $$ Ethanamide $$ Acetic acid amide $... 59 44 5000- 9.60 9.80 10.00 10.20 m/z 41.10 10.44% 41 01 tirr l 1 ‘ I ' ' ' 1 I “ ' ' I ‘ " I ‘ ‘ I ■ ■ • ■ i ■ •111 ■ • ■ ■ i ’ ■' ■ i - ■ ■ ■ i ■ ■ ■ ■ i ■ ■

miz-> 20253035404550556065 70 75 808590 N Abundance #500:2-METHYL-3,3-D2-AZIRIDINE 29 58 ’ 1 1 1 1 11 1 1 1 9.60 9.80 10.00 10.20 5000 m/z 42.10 9.01%

26 42

miz-> 0! • ■ i ■ ■ ■ ■ i < 111 ‘‘ I'' Mlil.. ..... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 I ■ ■ “ i ■1" i1 ■ ■ ■ i ■" ■ i ■ “ ■ i " '' i ■ ■

Abundance #9659:3-Pentanol, 2-methyl- (CAS) $$ 2-Methyl-3-pentanol... 59 A 9.80 10.00 10.20 9.60 m/z 83.90 8.79% 5000 31 73 A NNV A A /

55 27 69 42 45 niz-> 0 1111 ■ “ i •1 ■ ■ i H - 84 • ।111111 I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 pjakii TTT r ‘d.8 9.60 9.80 10.00 10.20

00839.D SCAN508.M Thu Jan 24 09:57:28 2002 Page 4

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