DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02016.D Vial: 4 Acq On : 26 Feb 2002 12:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 7 2-METHYL-3,3-D2-AZIRIDINE Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

9.91 0.09 ug/L 44657 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 9 2 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 3 ETHYLAMMONIUMCHLORIDE $$ Ethanam... 45 C2H7N 000075-04-7 4 4 PROPANE-2-13C 45 C3H8 017251-62-6 4 Abundance Scan 579 (9.910 min): 02016.D (-) m/z 59.10 100.00% 59

5000

45 0- ■।■■■■।■■' ■ । ■1'' ।111 ■ । ■ ■■11■■111 ■' ■ ■ । ■ ■ ■ ■ । ■ i '' ■ ■ i '' 1 11 152 1111 ■ ■ i11 ■ 111 ‘ ■ i m/ z M 9.60 9.80 45.00 WAAAM.. 10.00 10.20 15.25% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #500: 2-METHYL-3,3-D2-AZIRIDINE 23 58 M 5000 ' 1 '‘i 1 9.60 9.80 10.00 10.20 m/z 44.00 14.29%

mlz-> O-ri 1 1 ' rrr

Abundance 11 ■ ■11 ■ ■ ■' i1 1 '' i1 ■ ■ ■ i1'' ' i '1' ■ i 'r' ■ i1' ‘ ■ i1 1'11 ■1 ■ ■ i

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine ... 59 Ai TTT 9.60 9.80 10.00 10.20 5000 m/z 43.00 12.63% 42

N A m/z-> OTT 10 -1 "I 1* 20 30 40 50 60 70 80 90 100 110 120 130 140 150 i ' 1 ' ' i ' ' ' ' i 1 I '111 I ' ' 1 ‘ I ' ' 1 ' I W

Abundance #261: ETHYLAMMONIUMCHLORIDE $$ Ethanamine (CAS) $$ Ethylam... ■ ■ । - i 1 ■ ' ‘ i 3b 9.60 9.80 10.00 10.20 m/ z 41.10 12.57%

5000 45

0 —7l —3814 ■ i ■ ■' ■ i ■ ■ '' i ‘1 ■ ■ i 1'' ■ i ■ i ‘ ' 1 i ' 1 ' ■ i 111 r ■ ■ i11'1111 ■11 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 9.60 9.80 10.00 10.20

02016.D HP022102.M Wed Feb 27 08:34:33 2002 Page 9

NYC-WTC_000004537