GCMS analysis report for sample AE01636, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report . -Data File : C:\MSDCHEM\1\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Benzene, (2-methoxyethoxy)-... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 9.90 0.07 ug/L 31951 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, (2-methoxyethoxy)- $$ 1... 152 C9H12O2 041532-81-4 9 2 1-Propanamine (CAS) $$ n-Propyla... 59 C3H9N 000107-10-8 4 3 2-METHYL-3,3-D2-AZIRIDINE 59 C3H5D2N 030691-55-5 4

Al 4 DEUTEROACETONE 59 C3H5DO 004468-52-4 4 Abundance Scan 578 (9.899 min): 01636.0 (-) m/z 59.00 100.00% 59

5000 45 152

O+ 1 t ‘ ‘ ‘ ‘ I ‘ ‘ ‘ 1 ' ... 84.... TT-p 9.60 m/z 152.10 9.80 10.00 10.20 26.68% nz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #49049: Benzene, (2-methoxyethoxy)- $$ 1-Methoxy-2-phenoxy... 59 ........ .................................... 5000 77 94 9.60 9.80 10.00 10.20 31 152 45

+ m/z 45.10 26.51% 0 ■i•■■■i 197 120 A /z-> 20 30 1 ■ i • ■ ■ ■ i ■ 1 40 50 K) 70 • * i ■' ■' i ‘ 80 90 1 ‘ l 1 " ‘ I " ■■ V-. T, t 100 110 120 130 140 150 “ | “ . . | ■ ■ i ■ A Abundance #654:1-Propanamine (CAS) $$ n-Propylamine $$ Propylamine... 50 9.60 9.80 10.00 10.20 5000 42 m/z 44.00 20.61% YA U miz-> Of ■ i ■ • ■ ■ I ‘' ■ ■ i 20 30 40 -1 50 60 “ i' 70 ‘ ‘ I' ‘ ‘ ‘ i ‘ ‘‘ i ‘ ‘ 80 90 ‘ 11 " ‘ i'' • ‘ 11 ‘ ‘ ‘ i • • ■ ■ i ‘ 100 110 120 130 140 150 ' i'

Abundance #500:2-METHYL-3,3-D2-AZIRIDINE 1 'I • 1 29 58 9.60 9.80 ‘ 10.00 10.20 m/z 83.90 5.67%

5000-

42 M4 /z—> 0 11+4 20 30 1. Al... 60 40 50 11 ■ ■ ■ i ■ • ■ ‘ i ■ ■ • ■ i ‘ ‘ ‘ ‘ i ■ ■' ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ • ■ i1 ■ ‘ ‘ I ■ 70 80 90 100 110 120 130 140 150 9.60 9.80 10.00 10.20

01636.D HP022102.M Mon Feb 25 10:55:38 2002 Page 10

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