GCMS analysis report for sample AE01636, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report . ‘Data File: C:\MSDCHEM\l\5973N\02FEB21\01636.D Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 7 Ethanone, 1-cyclopropyl- (C... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.18 0.05 ug/L 21784 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Ethanone, 1-cyclopropyl- (CAS) $... 84 C5H80 000765-43-5 4 2 Furan, 2,3-dihydro-5-methyl- (CA... 84 C5H80 001487-15-6 4 3 Ethanone, 1-cyclopropyl- (CAS) $... 84 C5H80 000765-43-5 4 4 Furan, 2,3-dihydro-5-methyl- (CA... 84 C5H80 001487-15-6 4 Abundance Scan 249 (6.185 min): 01636.D (-) m/z 43.10 100.00% 43

5000

49 59 84 M—A U .. A 6.00 6.20 6.40 6.60 5.80 01 111 • “ ■ i ■1 “ 111'' 11"111' * i ‘ ■ r' i11'111' 1111 ■ • i ■ ■ ■ ■ । -' ■ • । ■ i1 ■ ■' । । ■ ■ • ■ । m/z 59.10 29.97% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3280: Ethanone, 1-cyclopropyl- (CAS) $$ Cyclopropyl methy... 4)3 69

5000 39 __5.80 6.00 6.20 _______ 6.40 6.60 27 84 m/z 83.90 22.03%

iz-> Abundance 01 '11111'J ।11111'11111 f 20 25 30 35 40 45 49 ‘ i ■ “ 11 • " • I ■ " ‘ i' “ 11 “ 50 55 55 60 65 70 #3349: Furan, 2,3-dihydro-5-methyl- (CAS) $$ 2-Methyl-4,5-... 1' 11''11111 trr.-Tp-.-TrT 75 80 85 90 MMMnMMhwwaidl 43 5.80 6.00 6.20 6.40 'iso' 5000 m/z 49.00 19.08% 27 31 39

69 84 W//WAwAAA 01 ■ ■ i ■ “ ' i ■ rrp ■11 “ ‘I■ " ' I' ‘ “ I' ‘ " I “ 111111111111111'11'1 Ti ■ f ■ ■' l niz-> 20 25 30 35 40 45 55 60 65 70 75 80 85 90 Abundance #3287: Ethanone, 1-cyclopropyl- (CAS) $$ Cyclopropyl methy... ■ i ■ • ■ ■ i ■ ■ • ■ i ■ ■ ■ ■ i • ■ • ■ i * ■ 43 5.80 6.00 6.20 6.40 6.60 69 m/z 51.00 3.10% 5000 84 A N AAA W A 27 38 oi ■ ■ i ■ ... 111 ■ • ।... > I > 11. । + .i...»11.1■ 1.... 1। ■ 53 " I'11111'1 H' " ' i " ■ ■ i niz-> 20 2530354045505560 65 70 75 80 85 90 5.80 6.00 6.20 6.40 6.60

01636.D HP022102.M Mon Feb 25 10:55:38 2002 Page 9

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