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GCMS analysis results for sample AE07974, April 18, 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE07974 conducted on April 18, 2002.

NYC-WTC_000047564–000047576

Folder label: “GCMS X 4/4/02 A 4/15/02

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Scanned page image, NYC-WTC_000047571
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020415\07974.D Vial: 14 Acq On : 15 Apr 2002 9:26 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Furan, 2,3-dihydro-5-methyl­ Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.78 0.27 ug/L 212887 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, 2,3-dihydro-5-methyl- 84 C5H80 001487-15-6 5 2 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 5 3 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 4 4 2-Amino-octadec-7-ene-1,3-diol m... 323 C19H38BN02 1000143-52-3 4 Abundance Scan 118(3 773 min): 07974 D (-111) (-) m/z 43.30 100.00% 43 I 40 5000

84 LLAM—LalA 49 340 3 60 3.80 4.00 4.20 ..................... 35... 1), —HH 0 T’TTI’UIUIUTTOUOOTTTCCTTTTTLT r "11" " i " | 88 i" " r '111 m/ z 40.20 52.47% /z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #110041: Furan, 2,3-dihydro-5-methyF 43

5000 84 3.40 3.60 3 80 4 00 4 20 39 m/z 84.20 19.51%

kodwwi/"Mwy 27 55 50 69

n/z-> ol " r " 11" " r ■ " i111' i11111' TIH TT‘—#H 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 ......I,..... 80 85 90 95 i *'1 ■ r '' > । "

Abundance #109806: Ethanone, 1-cyclopropyl- 43 69 3 40 3 60 3 80 4.00 4 20 5000- m/ z 83.20 10.54% 39 15 27 84 12 | 18 31 36 50 55 58 62 65 0 mmPTPTTTTTHTT ......... .. ............... I.............. ' i' ■'' r' ■ n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109805: Ethanone, 1-cyclopropy 43 69 _A_L 340 3 60 3.80 4 00 4.20 m/ z 49.20 10.09% 5000 39 84 Moy/Me 27

n/Z-> 0 ■ i" ■' ।' 31,361+ 46 50 55 58 62 65 ■11" 1 ■ | ■ 7. ■ । । ■ 1 11177811 . ..... 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3 40 3 60 3 80 4 00 4 20

07974.D 041202SCAN.M Tue Apr 16 13:44:36 2002 Page 4

NYC-WTC_000047571

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NYC-WTC_000047571Source: NYC Law Department, mirrored locally

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