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GCMS analysis results for sample AE10609, May 10 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.

NYC-WTC_000045643–000045661

Folder label: “GCMS X 5/3/02 A 5/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050702\10609.D Vial: 12 Acq On 7 May 2002 10:06 pm Operator: Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Ethanone, 1-cyclopropyl- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.73 0.25 ug/L 193090 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 5 2 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 • 3 Furan, 2,3-dihydro-5-methyl- 84 C5H80 001487-15/ 5 4 3-Buten-2-one, 3-methyl-____________ 84 C5H80 000814-78-8 4 Abundance Scan 110 (3.725 min): 10609.D (-108) (-) m/z 43.10 100.00% 43 _/

5000 51 84 37 55 I I I [ I I I I [ I I I I I I I I I J I 1—I I I

m/z-> ′′′′′′ 5 10 I''1 ’ I T 4 al....... 47

15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 58 88 r 1 " r 11' r ■ m/z 3.40 3.60 42.10 3.80 4.00 29.66% Abundance #109805: Ethanone, 1 -cyclopropyl- 43 69 / A 5000 11 39 84 3.40 3.60 3.80 4.00 m/ z 51.00 28.59% 27 +31.3644 46 50 55 58 6265 ...... I"1'!................ +7781 11" ' i " 111 ■1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109804: Ethanone, 1-cyclopropyl- 43 69 1 1 1 I ‘ ' I ' ‘ 1 ' 1 1 1 ' ' I 1 1 1 1 I 3.40 3.60 3.80 4.00 5000 m/z 84.00 28.59% 84

27 39 mkolArooo. m/z-> 5 r ■ ■ 11' 1218, IIdpunanpaldit 1 31 36, , 46 50 5558 6366 TTTTTHTwuur 1111111 I I I I I I I 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 I I I > > I I I I I I > I

Abundance #110041: Furan, 2,3-dihydro-5-methyl- 1 1 1 i ■ ■ ' 1 i 1 1 ■ 1 । 1 ■ 1 1 i 1 1 1 1 i 43 3.40 3.60 3.80 4.00 m/z 37.00 20.05%

5000 84 39 27 55

m/z-> l +50L 69

5 10 15 20 25 30 35 40 45 50 55 60 65 70 i " 111' 11111 I’*’’}’’ 75 80 85 90 i " " i " " i11 95 IWJ NF, 3.40 3.60 3.80 ' 1 1 1 4.00

10609.D 050102.M Thu May 09 09:13:54 2002 Page 5

NYC-WTC_000045652

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GCMS analysis results, sample AE09968, May 2002 · Box DEP Box 25

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Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996

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