GCMS analysis results, sample AE06334, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6334.D Vial: 18 Acq On 9 Apr 2002 2:41 am Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 4-Penten-2-one Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 5.59 0.11 ug/1 72007 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 4-Penten-2-one 84 C5H80 013891-87-7 4 2 4-Penten-2-one 84 C5H80 013891-87-7 1 3 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 1 4 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 1 Abundance Scan 427 (5.588 min): 6334. D (-423) (-) m/ z 43.10 100.00% 43

5000

49 84 5.20 5.40 5 60 5.80 6.00 40 01 11 U ■" ■ i1 ■ ■11 ■ ■" r ■" I " 11111111' i ■ ■ ■ 11■ • ‘■ i■ ■ ■ ■ i>■ ■ ■i■■■■i■■■■i।■1•i।■■■■t■ • ■ ■ i m/z 49.05 6.14% m/z-> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #4029: 4-Penten-2-one 43 MlMwyAaaMANM/L 5000 5.20 5.40 5.60 5.80 6.00 15 39 m/z 84.00 5.27%

mlz-> 0 " I"" l ■ " ■ I ■ i । । | r I I I I’2731 12 I 1 1 ! | I I r I [ I I I

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 5053 69 11 ■1 ■ ■ 11 ■1' 11"1111" 111'11" ■ ■ i1'1 ■ i ■ 84 mm "DMM-./NVN/MMWM,// Abundance #109203:4-Penten-2-one 43 ■ i 1 ■ ■ ' i ' 1 5.20 5.40 5.60 5.80 6.00 5000 m/z 40.05 2.56%

28 39 84

m/z—> ol "Ii 5 -HFl - 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 r i" •r i

Abundance #109805: Ethanone, 1-cyclopropyl- 43 69 5.20 5.40 5.60 5.80 6.00

5000 39 84

27

m/z- > 0 -..... -........ 364+ 46 50 5558 6265 +81— I ) । । t i | I i h | i । । । TT i i । । i । । 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ‘ i " '11

6334.D SCANAPR0902.M Tue Apr 09 15:20:22 2002 Page 6

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