GCMS analysis results, sample AE06334, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6334.D Vial: 18 Acq On 9 Apr 2002 2:41 am Operator: McLean Sample 3/18 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 5 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.69 0.36 ug/1 330819 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 N-(Trifluoroacetyl)-N,O,O',O''-t... 553 C22H42F3NO4Si4 1000072-26-7 37 4 Noradrenaline tetraTMS 457 C20H43NO3Si4 068595-65-3 37 Abundance Scan 1976 (14.689 min): 6334.D (-1968) (-) m/z 73.10 100.00% 73

5000 267 355

1 1 i ■ ■ ' ' i । ■ i ■ ■ • ■ । । 14.40 14.60 14.80 15.00 0-1 1 ■ 40I । ■ i ‘ ■ । । । । * । < । । । । । > > । । > i . ' j < > । । /iI । । । । । । । । । f । । । TIT । । । । m/z 267.00 46.70% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 267 5000 ■ i 1 1 1 1 i 1 1 1 ' i 1 ■ ' 1 । ■ ' 14.40 14.60 14.80 15.00 m/z 355.00 45.40% 45 207 323 0- -4 , — tt tT — —+ m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

1 I 1 1 14.40 14.60 14.80 15.00 5000 267 m/z 356.10 16.37% 355 45 103 133 165 193 223 , 0-44 TTTTTTTTrf :293 323, 1 .... .... miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #27961: N-(Trifluoroacetyl)-N,O,O’,O"-tetrakis(trimethyls... 73 14.40 14.60 14.80 15.00 m/z 267.90 11.61% 355 5000

45 116 14? 193 236 267 538 0U 1 > 1 i 1 1 ' ■ i ■ ‘ 1 ' I ' 1 1 ' I 1 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00

6334.D SCANAPR0902.M Tue Apr 09 15:20:24 2002 Page 7

NYC-WTC_000039403