GCMS surrogate recovery data for sample AE07765, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020410\05286.D Vial: 12 Acq On : 10 Apr 2002 8:43 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.69 0.45 ug/1 424019 Naphthalene-d8 15.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9 64 4 N-(Trifluoroacetyl)-N,O,O',O',-t... 553 C22H42F3NO4Si4 1000072-26-7 37 Abundance Scan 1975 (14.683 min): 05286.D (-1959) (-) m/z 73.10 100.00% 73

5000 267 355

40 14.40 14.60 14.80 15.00 0 m/z 267.00 42.82% m/z-> 50 100 150 200 250 300 350 400 450 A Abundance #115315: Cyclopentasiloxane, decamethyl- 73 355 267 5000 1 1 i ■ ■ 14.40 14.60 14.80 15.00 m/z 355.00 41.87% 45 0- i t 1 i 1 — ———— 207 । 4- 323 L ■ l ■ ■ ■ • i ■ 1‘I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #115273: Cyclopentasiloxane, decamethyl- 73

14.40 14.60 14.80 15.00 5000 267 m/ z 3 5 6.00 14.43% 355 A 45 01 — 96 133 165 193 TT ' > "IT 223, 422931Bduf 323 i 11" ■ i ■ ■ • ■ i ■ ■ • ■ । m/z-> 50 100 150 200 250 300 350 400 450 Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet... 73 14.40 14.60 14.80 15.00 m/ z 2 68.00 11.79% 5000 207

133 281 355 0 — 1 103 I 177_1 !j11 i ■ 1 1 , 253] | ' 1 1 'TIT i ■ 327 |, 377399 429 ‘ 1 ” i I ' 1 1 11 1 1 ‘ 11 1 i ‘ 489 1 1 i m/z-> 50 100 150 200 250 :300 350 400 450 14.40 14.60 14.80 15.00

05286.D SCANAPR0902.M Thu-Apr 11 14:08:30 2002 Page 4

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