GCMS analysis report, sample AE07569, April 2002

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Data File C:\MSDCHEM\l\DATA\020403\07569.D Vial: 17 Acq On 3 Apr 2002 11:52 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 14.69 0.39 ug/1 365128 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 4 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H44O6Si7 019095-23-9 64 Abundance Scan 1976 (14.689 min): 07569.D (-1965) (-) m/z 73.10 100.00% 73

267 355 5000

40 14.40 14.60 14.80 15.00 0- e 1 " i 1 1 1 ' 1 1 " 1 i 1 iri i 111 " < I ■■ ■ 1111"* IUUE’I’’*’I’’II’NU’TI ’SstI’ 1111111111 n T’t m/z 355.00 59.39% m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #103462: Cyclopentasiloxane, decamethyl- 355

73 267 5000 14.40 14.60 14.80 15.00 m/ z 2 67.00 54.70% 4 28 45 o1 i ‘ " 1 r 1" i'" 1 i " TTap108 133 154 176193 223 249 [ 293 r i 323 11vyrsd1o p 11111, r, । f .. 1.11 j > । r. । i "'I' Fil1 ■ । Vi i i ‘f i i i Tp-r n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73

355 14.40 14.60 14.80 15.00 267 5000 m/z 3 56.00 20.60%

m/z-> I 45 o1 I‘‘‘I‘IINASESIARSIf// 0 207 mWmppt 249 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 323 —

Abundance #115273: Cyclopentasiloxane, decamethyl- 73 14.40 14.60 14.80 15.00 m/z 268.00 13.52% 5000 267 355 45 28. 96 115133 165 193 0-p 1" i ■1" i*'11111 Aycttyttonynoduyoveu |T M rushy M , rt i , 223 24,9 I tt > I r 293 323 t i ■'" r " 1 lTI "‘I " '^l " m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00

07569.D SCAN020403.M Thu Apr 04 10:44:29 2002 Page 5

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