GCMS analysis report, sample AE07520, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\0402LB.D Vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Cyclopentasiloxane, decamet... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

14.69 0.38 ug/1 337395 Naphthalene-d8 15.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 83 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 4 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 Abundance Scan 1976 (14.689 min): 0402LB.D (-1968) (-)■ m/ z 73.10 100.00% 73

267 355 5000

3” I ' | । । i i । f i i । । i -'I_'f I ' ]' I |

14.40 14.60 14.80 15.00 0- I‘rrTT‘ETTTETT‘T‘T71TTTTTTETT‘‘TT‘11‘1‘1‘1111‘11111111111110111111111111111‘111117 1’’ m/Z 355.10 53.56% m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #103462: Cyclopentasiloxane, decamethyl- 355

73 267 5000 14.40 14.60 14.80 15.00 m/z 267.00 51.52% 4 28 45108 133 154 176193 223 249 [ 293 323 01 I"111 ITWIIImIIumori‘ TTTTTT m/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73 i_"i । r r । । '। i i । । i । । ”i—|" 1" 'i'

355 14.40 14.60 14.80 15.00 267 5000 m/ z 3 56.00 21.51%

45 207 249 323 0-T ———————————— TP L I " " I' Ttm 1 n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73 14.40 14.60 14.80 15.00 m/z 268.00 14.28%

5000 267 355 45 28 1 TumTTTp O—T I i r i I i i | | I 96 115133 165 193 223 249 t 293 323 11 1 1 | i if [ 11' r 111 r 11' i '11'I ■111 r ' ’ 1 i 1 1 1 1 i 1 1 1 1 i ■ 1 1 1 i ■ ‘ m/z~> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00

0402LB.D SCAN020403 .M Thu Apr 04 10:14:21 2002 Page 5

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