GCMS analysis report, sample AE07520, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\0402LB.D Vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2,3,4,5-Tetrahydropyridazine Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 3.31 0.16 ug/1 104836 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3,4,5-Tetrahydropyridazine 84 C4H8N2 000694-06-4 2 2 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 2 3 Formamide, N-(cyanomethyl)- 84 C3H4N20 005018-27-9 2 4 Pentane, 3-methylene-________________ 84 C6H12 000760-21-4 2 Abundance Scan 40 (3.314 min): 0402LB.D (-39) (-) m/z 84.00 100.00% 84

5000

47 TT 1111' 1 1' " I I' ■ ■ 111 11 11 3.20 3.30 3.40 3.50 3.60 3.70 Oh ‘11131111/111111111717110111111 i ■ ■'11 ■11 r i m/z 47.10 17.23% m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 Abundance 28 #33489: 2,3,4,5-Tetrahydropyridazine 80 85 84 90 95 । AWWA MAM 5000 55 i''' ■ i TT ■ i' ■1

41 3.20 3.30 3.40 3.50 3.60 3.70 69 oh ■11111 ■ ।11111 > ' ' 1 1 1 1 I ■ ■ ■ ■ । ■ i' ■'111 ' ■ ■ r ■ r 1 1 ' i' '' ■ i m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109805: Ethanone, 1 -cyclopropyl- 43 69

5000 39 84

27 Oh m/z-> 15 20 -3139 46 50 55 58 62 65 I | r i t t | I i I I | i i i । । I I i i । f rr —7781 I 1 ■' ■ i1 1 1 1 i 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #541: Formamide, N-(cyanomethyl)- 29

84 5000 55

40 36 43 Oh ■r i • ■ > ■ i ■ ■ +r —HHH TH 58 61 66 I i~ । i , . 1711 111 FIn 111 11111 > i Tm m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

0402LB.D SCAN020403.M Thu Apr 04 10:14:18 2002 Page 4

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