GCMS analysis report, sample AE07569, April 2002

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Data File C:\MSDCHEM\l\DATA\020403\07569.D Vial: 17 Acq On 3 Apr 2002 11:52 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 4-Penten-2-one Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.42 0.11 ug/1 75455 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-Penten-2-one 84 C5H80 013891-87-7 3 2 Ethanone, 1-cyclopropyl- 84 C5H80 000765-43-5 3 3 Acetic acid ethenyl ester 86 C4H602 000108-05-4 3 4 2-Butyne-1,4-diol 86 C4H602 000110-65-6 3 Abundance Scan 58 (3.420 min): 07569.D (-56) (-) m/ z 43.10 100.00% 43

5000

40 . ......... 11 .................... 51 84 3 20 3.40 3.60 3.80 Of 1' r " 11" " i" " i ■1" i1" 111 ‘ ■111 i f i । I । । i TT i | > i i I | i > i i । i i > i । i TT m/z 40.10 21.30% n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109203: 4-Penten-2-one 43

5000 320 3.40 3.60 3.80 m/z 51.00 14.27% 28 39 84

/z-> Abundance 01 - hm P 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #109806: Ethanone, 1 -cyclopropyl- --- wo""MMwr, "*

43 69 320 3.40 3.60 3.80 5000 m/z 84.00 13.65%

12 15 | 18 27 31 36 0 " r " 11" 11111111' TTHHTTT 39

50 5558 6265 11" 11111111" " I " " I ■ " Pt TTTTT 84 .Ww Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #109145: Acetic acid ethenyl ester ■ । ‘ । 1 ■ ■ ■ i ' 1 1 1 i 1 1 1 43 3 20 3.40 3.60 3.80 m/z 86.00 2.79% 5000 v/""Whuado 27 0 ,1 ,31 3740) 11'"11 5760 71 86 T‘"' i" " I ■1" I" " i'111 r1111'1 ■11 ■ ■1 ■ 11 1 i 1 ' ' ' i 1 ■ ' ■ I ' 1 1 ' 1 1 Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.20 3.40 3.60 3.80

07569.D SCAN020403 .M Thu Apr 04 10:44:24 2002 Page 3

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