GCMS analysis results for sample AE08066, Apr 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08066.D Vial 23 Acq On : 16 Apr 2002 4:47 am Operator Nefliu Sample : sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Acetic acid ethenyl ester Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.78 0.29 ug/L 206621 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid ethenyl ester 86 C4H602 000108-05-4 9 2 2-Pentanone 86 C5H10O 000107-87-9 9 3 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 9 4 2,3-Butanedione 86 C4H602 000431-03-8 7 Abundance Scan 118 (3.772 mm) 08066.D (-101) (-) m/z 43.30 100.00% 43

5000 49 86 AA—AGAAA 3 40 3 60 3 80 4.00 4 20 01 ................ 361 1 rrm" 1 1 । I । 1 1......Hill ‘‘‘‘I’’ m/z 49.20 31.93% n/z- > Abundance 10 20 30 40 50 60 70 80 90 #110103. Acetic acid ethenyl ester 43 100 110 120 MMAMMMp 5000 340 3.60 3.80 4.00 4 20 86 m/z 86.15 19.64%

n/z-> 15 0+ ......i1......... 10 20 27

30 4 ................................. ............ ... . 40 50 60 70 80 90 100 110 120 Mpouw/MMuny Abundance #110097 2-Pentanone 43

340 3.60 3 80 4 00 4 20 5000 m/z 51.20 16.27%

27 I 58 71 86 MeryW"MMPNMmo" n/z- > ol -L4 10 20 30 40 +r 50 - 60 70 T-r-J-H-TT-r-f-r-r 80 90 100 110 120 Abundance #1082: Ethanol, 2.2-dichloro- 31 340 3.60 3 80 4 00 4.20 m/ z 84.10 15.79% 5000 MAaAPHWwy 0 25 , 37 43 49 55 61 70 77 83 96 103 114 ■ ■ l ‘ ■ l ■ 1 r' p 1 ' r1 11-1 I'11 111‘n ■ ■ । ■ । । ■ /i . । । । । । । 11»> I • > Tl/Z-> 10 20 301 40 50 60 70 80 90 100 110 120 3 40 3.60 3 80 4 00 4 20

08066.D 041202SCAN.M Tue Apr 16 13:55:43 2002 Page 4

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