GCMS analysis report, sample AE07520, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\0402LB.D Vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 trans-2,3-Methylenedioxy-b-... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

41.45 0.17 ug/1 122553 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 trans-2,3-Methylenedioxy-b-methy... 207 C10H9NO4 086029-47-2 5 2 2H-Indazol-3-amine, 2-methyl- 147 C8H9N3 1000142-18-7 2 3 1,3,2-Benzoxazaborole , 2-ethyl-2... 147 C8H10BNO 129363-62-8 2 4 Pyrido[2,3-d]pyrimidin-4(1H)-one 147 C7H5N30 024410-19-3 2 Abundance Scan 6531 (41.453 min): 0402LB.D (-6514) (-) m/ z 73.10 100.00% 73 147 40 221 207 5000

1 ' i ■ 41.20 41.40 41.60 41.80 0 i ■ ■ m/z 147.00 84.19% m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #126466: trans-2,3-Methylenedioxy-b-methyl-b-nitrostyrene 77 103 147 207

51 5000 91 39 41.20 41.40 41.60 41.80 63 119 131 m/z 40.10 78.29% —— 1 160 179 ।

m/z-> Ot। i ■ 1 ■ - i ■ ■ ■ ■ । 20 40 60 ■ JU100Ui120 80 140 160 ”...,200.I..... I180 220 Abundance #65968: 2H-lndazol-3-amine, 2-methyl- 147

41.20 41.40 41.60 ■41.80

A 5000 m/z 221.10 73.97% 77 104 39 51 65 ।। 92 118 132 I ■ ■ 1 ■ ■ ■ 1 । ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ 0 i 1 ■ ' T 1'' '' 1 "I" ■ ■"1 ' "' i'I' m/z-> 20 40 60 80 100 120 140 160 180 200 220 Abundance #66062:1,3,2-Benzoxazaborole, 2-ethyl-2,3-dihydro- TIT 1 ■ 1 ■ ■ r' 1 * ■ 1 1 1 ' 147 41.20 41.40 41.60 41.80 119

A m/z 207.00 60.38%

5000 132 27 40 52 63 77 9,1 105 . 0 । । > । I . . I , । T , । । , "I , । 1 । । "ll । Tt -------------------- 1 I ' ' 1 1 I m/z-> 20 40 60 80 100 120 140 160 180 200 220 41.20 41.40 41.60 41.80

0402LB.D SCAN020403.M Thu Apr 04 10:14:23 2002 Page 6

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