GCMS analysis results, sample AE07519, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07519.D Vial: 15 Acq On 4 Apr 2002 8:00 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 2,5-Dimethylbenzoxazole Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

43.83 0.10 ug/1 68461 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,5-Dimethylbenzoxazole 147 C9H9NO 005676-58-4 2 2 1,3,2 -Benzoxazaborole, 2-ethyl-2... 147 C8H10BNO 129363-62-8 2 3 2H-Indazol-3-amine, 2-methyl- 147 C8H9N3 1000142-18-7 2 4 1H-Inden-1-one, 5-amino-2,3-dihy... 147 C9H9NO 003470-54-0 2 Abundance Scan 6935 (43.826 min): 07519.D (-6928) (-) m/z 73.10 100.00% 73 40 147 207 5000

43.40 43.60 43.80 44.00 44.20 0 ' ‘" r "' r "11r r" r1" 1" " r "11111111" 1 r1111 1" " r' " 1" " I"'' I"'' I"'' 11"' I'1'' I" " Im m/z 147.10 68.48% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #65977:2,5-Dimethylbenzoxazole 147

78 5000 43.40 43.60 43.80 44.00 44.20 106 51 m/ Z 40.10 63.24% 15 27 39 | 91 63 I 118 132. 0 "i"'''r Ttpl mt i’ "'h'"-I1 "'i" pmmmmm m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #66062:1,3,2-Benzoxazaborole, 2-ethyl-2,3-dihydro- 147 119

43.40 43.60 43.80 44.00 44.20 5000 m/z 207.00 52.05% 132 J 27 40 52 63 77 91 105 0 " i" " i" i‘ "" I1 ■ ■ rt’lh111 r‘r 111 rT "'I 1111 TT m I 1" 11" " 1" " 1" " 1" " 1'"' 11 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #65968: 2H-lndazol-3-amine, 2-methyl- 13tr 1 ’ i ' ' 147 43.40 43.60 43.80 44.00 44.20

5000 77 104 39 51 65 118 132 0 | " " I U I I | I > rI’r’m Hr | I'l'l , ill.i .... Hi92 HHmmm mmmmmmmmmm Tl/Z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210

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