GCMS analysis report, sample AE07568, April 2002

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Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

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NYC 9/11 Public Portal Document

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 14 2-(2,6,6-Trimethylcyclohex-... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 44.78 0.41 ug/1 299198 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-(2,6,6-Trimethylcyclohex-l-eny... 222 C14H2202 1000185-64-1 9 2 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 3 3 5H-Pyrano[2,3,4,5-lmn]phenanthri... 221 C14H7N02 004733-28-2 2 4 2H-Indazol-3-amine, 2-methyl- 147 C8H9N3 1000142-18-7 2 Abundance Scan 7097 (44.778 min): 07568.D (-7087) (-) m/z 73.10 100.00% 73 147 221 5000 207 281

44.40 44.60 44.80 45.00 45.20 40 0 I""I"' m/z 147.10 68.62% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66034: 2-(2,6,6-Trimethylcyclohex-1-enyl)cyclopropanecarb... 147

107 5000 93 207 121133 175 44.40 44.60 44.80 45.00 45.20 41 55 79 163 m/z 221.10 57.38% , 222

n/z-> 0 AullLt 1444+94 20 27

40 60 67

80 100 120 140 160 180 200 220 240 260 280 Abundance #1079: Adenosine, 2-methyl- 31

44.40 44.60 44.80 45.00 45.20 5000 45 m/z 207.00 39.68% 59 74 149 1 78 -40dl.6014$80 100 120 140 160 180 200 220 240 260 280 m/z-> Abundance Ot i ' ■ :20 86 108120 133 i 163 | 192 206 239251264 281 fit r i i 1“ i fr । । 1" । । -i-i । 11" i ri FFITI । i i i i । 1n । FUmIm-rem

#87915: 5H-Pyrano[2,3,4,5-lmn]phenanthridin-5-one 221 Il | I [ fl I I I I I I I

44.40 44.60 44.80 45.00 45.20 m/z 281.00 35.28% 5000 A 193 164 39 68 138 ________ i_________ ii h____________________________ h_________ 0 r^| ' ' l ' । ■ r । > । । । 1 • । ri'i I I I......... I i i i I | ■ ' i ■ ■ ' ' i ' ■ 1 ' i ' ' ' ' i ' ■ ■ ■ i ' ■ TT n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 44.40 44.60 44.80 45.00 45.20

07568.D SCAN020403 .M Thu Apr 04 10:30:40 2002 Page 16

NYC-WTC_000047214

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