GCMS analysis results, Sample AE08269, April 22, 2002

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GCMS analysis report for sample AE08269 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048436–000048455

Folder label: “GCMS X 4/9/02 A 4/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08269.D Vial: 25 Acq On : 18 Apr 2002 5:10 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 1H-Indene, 2-phenyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

22.64 0.33 ug/L 600053 Phenanthranene-dlO 23.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1H-Indene, 2-phenyl- 192 C15H12 004505-48-0 59 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59 3 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 59 4 5H-Dibenzo[a,d]cycloheptene 192 C15H12 000256-81-5 58 Abundance Scan 3329 (22.639 min) 08269 D (-3323) (-) m/z 192.05 100.00% 152

5000-

Ttv --- 82 96 146 160 . 22 40 22 60 22 80 23 00 42 52 66 118 11, 11111J > 1111111.।... i ll ., ।,.

n/Z-> 0- ... ....... . 4 ''I....... . ■ ■ 11' ■ ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m/z 191.10 18.11% Abundance #125852' 1H-lndene, 2-phenyl- 192

....... . . 5000 22 40 22.60 22 80 23 00 m/z 193.00 15.06%

m/z— > 27 39 oV my 20 51 63 75 83 96 ’I’ ‘I"'1'I 115 139 152 1 0 126 165 | 176 l I11'........... I........ .......... ........... .' I' ■1' I 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844 Anthracene, 2-methyH- 102 , .... . 22 40 22.60 22 80 23.00 5000- m/z 96.00 14.93%

o_ 96 165 63 74 . ....... ....... ............................. ' i1 r' Htou nz-s 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81033: Phenanthrene, 9-methyl- 19 2 22.40 22.60 22 80 23.00 m/z 146.00 14.75%

5000

86 165 i i

n/z-> 29 39 0 IWI9I—B*nVUTu 51 +115,126,139.152.p47fl 63 75 83 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 ■ i'1 - 22 40 22 60 22 80 23 00

08269 .D 041702SCAN.M Thu Apr 18 10:02:30 2002 Page 13

NYC-WTC_000048452

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