GCMS analysis results for sample AE08489, May 2002

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Laboratory report documenting GCMS analysis of sample AE08489 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048672–000048682

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08488.D Vial: 25 Acq On : 20 Apr 2002 7:45 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C: \DATABASE\nist 98.1 ********************************************************************* Peak Number 3 Phenanthrene, 9-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.28 ug/1 552477 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 45 2 Anthracene, 9-methyl- 192 C15H12 000779-02-2 42 3 Thiocyanic acid, 2-benzothiazoly. .. 192 C8H4N2S2 006011-99-0 42 4 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 Abundance Scan 4768 (31.094 min): 08488.D (-4757) (-) m/z 192.10 100.00% 192

5000

40 82 96 146 160 30.80 31.00 31.20 31.40

iz-> I 51 TWTHTgo 70 | mil... ......... 4,......... ... ll 20 30 40 50 60 70 80 90 1CX) 110 120 130 140 150 160 170 180 190 200 m/z 146.10 14.74% Abundance #81033: Phenanthrene, 9-methyl- 15 2

5000 30.80 31.00 31.20 31.40 m/z 193.00 13.60% 96

miz-> 29 39 51 63 74 83 115 126 139 152 TIWIPmuamn—mmugTHhmr 1B99unuunnmn—u—nftnr ‘ I‘1 20 30 40 50 60 70 80 90 100 110 120 130140 150 160 170 180190 200 1,1764 Abundance #125848: Anthracene, 9-methyl- 192

30.80 31.00 31.20 31.40 5000 m/z 191.10 13.20% 96 2 27 39 , i51p ,., 1163’... ।. ri. 82 , (. 11... ,| 115 126 139 152 1? 176 „|| iT, IT] i rp > 111 IrT) 11 ri 111 ‘ ‘ 11 ■ i rli 111 i’i'i i p i i 1111 i'lt up, miz-> 20 30 40 50 60 70 80 90 100 110120 130140 150 160170 180190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 152 30.80 31.00 31.20 31.40 m/z 12.05% 5000

....... 45............................................... I.... > 11 > > ■ 11 ■ > > । > li > । > i > > ।, t > > । < > 1 > ! I ,, > | , I 11 ■ i i I 11 ■ 11 11 ( 1111 I,, । 11111 1111"| ■ 11 11 111 > ITTTTT . > p i ’ ’ I * ' v-r-r-r-r n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 2(X) 30.80 31.00 31.20 31.40

08488.D SCAN020418.M Thu May 02 12:03:39 2002 Page 5

NYC-WTC_000048680

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Document fragment from DEP Box 27, April 2002 · Box DEP Box 27

NYC-WTC_000048683

Single page document fragment from the DEP Box 27 archive folder dated between April 10 and April 15, 2002.

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