GCMS analysis results for sample AE08486, May 2002

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Laboratory report documenting GCMS analysis of sample AE08486 conducted on May 7, 2002, by analyst DLV.

NYC-WTC_000048647–000048659

Folder label: “GCMS X 4/10/02 A 4/20/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020419\08484 .D Vial: 21 Acq On : 20 Apr 2002 3:49 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\ni st 9 8.1 ********************************************************************* Peak Number 4 2,4-Diamino-6-(hydroxymethy... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.33 ug/1 767990 Phenanthrene-dl0 31.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 59 2 lH-2-Indenone,2,4,5,6,7,7a-hexah... 192 C13H20O 1000196-69-5 42 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 42 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 Abundance Scan 4767 (31.088 min): 08484.D (-4751) (-) m/z 192.10 100.00% 192

5000

40 96 146 160 30.80 31.00 31.20 31.40 152 66 82 1 120 > 11111 > 111 ■, | < i*i 111111111111111,11111111 ri j 111111 ■ I rr 111 1i111 "•I. I “' ''I'1 ■“! l ■ "‘I1 - m/z 146.10 16.81% miz-> 20 30 40 50 60 70 80 90 100110120130140150 160170180 190 200 Abundance #125821:2,4-Diamino-6-(hydroxymethyl)pteridine 43 19/2 163

5000 28 30.80 31.00 31.20 31.40 53 m/z 191.10 15.42% 1 77 92 106 121 133 146 175 . miz-> 4 ltmtmlhmmp n | > rl [ ii > i । 11 > ij i i i 11 ।—। 11 11 । 11 1111 i । 11 n । i । 111 > । > 11 > 1 il rr 11 11 rrr i l r rr i [ ere | > 11 rrr i ij n 20 30 40 50 60 70 80 90 100110120130140150 160170180 190 200 Abundance #80945:1 H-2-lndenone,2,4,5,6,7,7a-hexahydro-3-(1-methylet.. 192 - 149 30.80 31.00 31.20 31.40' 177 5000 m/z96.00 13.87% 41 93 107 121 135 164 55 67 79

m/z-> 27 mJI Ji 11 A. | „Al, . l l I III । a 1, 4 I'l'i jl'i 11 i-il 2030405060 70 8090 100110120130 140150 160170180190 200 +u 1l I, pn I’, ।, 11 jl L 1111,

Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 1512 30.80 31.00 31.20 31.40 m/z 40.10 12.46% —ARMW—VARWWw

50001

45 ill 90 198 122 134 148 160 ( qpmmmmmmmmmmmmmml 4*I8A+I*I‘I-‘1I /z—> 20 30 40 50 60 70 80 90 100 110120130140150160170180190 200 30.80 31.00 31.20 31.40

08484.D SCAN020418.M Thu May 02 11:45:27 2002 Page 6

NYC-WTC_000048656

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GCMS sample analysis report AE08483, May 7 2002 · Box DEP Box 27

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Gas chromatography-mass spectrometry results for sample AE08483 including surrogate recovery data.

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