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GCMS analysis results for sample AE10207, May 2002

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Laboratory report detailing GCMS analysis of sample AE10207 conducted on May 17, 2002, including surrogate recovery data.

NYC-WTC_000024305–000024318

Folder label: “GCMS X 5/1/02 A 5/9/02

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Scanned page image, NYC-WTC_000024312
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020509\10207.D Vial: 9 Acq On 9 May 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 2,4-Diamino-6-(hydroxymethy... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.09 0.34 ug/1 53102 Phenanthrene-dl0 31.73

Hit# of 5 Tentative ..ID MW MolForm CAS# Qual

1 2,4-Diamino -6-(hydroxymethyl)pte... 192 C7H8N60 000945-24-4 59 2 Thiocyanic acid, 2-benzothiazoly. . . 192 C8H4N2S2 006011-99-0 53 3 [1] Benzopyrano [3, 4-b] [ l ] benzopyr. . . 342 C19H1806 003564-85-0 45 4 Phenanthrene, 8-methyl- 192 C15H12 000883-20-5 42 Abundance /Scan 4768 (31.094 min): 10207.D (-4754) (-) m/z 192.10 100.00% 192

5000

PTTTTTT i 1 'f' i ■' . 54 96 । 146 30.80 31.00 31.20 31.40 ... 342................ 542 —r d,—U44tpd"p"el i11'[ I । 'l । । । । । i । m/z 191.10 17.12% iz-> 50 100 150 200 250 300 350 400 450 500 Abundance #80958: 2,4-Diamino-6-(hydroxymethyl)pteridine 43 163 192 5000 1 J ' i ' ■ ■ 1 i 1 ' 30.80 31.00 31.20 31.40 68 m/z 146.20 14.25% 1411.974741 1 ■ । 1 1 ■ ■ । 1 ■ ■ 1 । niz-> 50 100 150 200 250 300 350 400 450 500 Abundance #80870: Thiocyanic acid, 2-benzothiazoIyl ester 192 1 P.... h,. 30,80 31,00 31,20 31.40 5000 m/z 193.10 13.51%

45 . ................... ...................... . 50 100 150 200 250 ' ' 300 350 ' 400 450 500 ' miz-> Abundance #81044: [1lBenzopyrano[3,4-b][1]benzopyran-12(6H)-one, 6a,... 192 ..AT ‘I‘ 30.80 31,00 31.20 31,40 m/z 96.20 11.81% 5000 342

m/z—> ----- 50 100 121 149

150 200 250 300 350 400 450 500 L 30.80 31.00 31.20 31.40

10207.D SCAN020507.M Tue May 14 14:22:11 2002 Page 4

NYC-WTC_000024312

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NYC-WTC_000024312Source: NYC Law Department, mirrored locally

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