GCMS analysis results for sample AE10207, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020509\10207.D Vial: 9 Acq On 9 May 2002 6:32 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Phenanthrene-diO Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 31.96 0.34 ug/1 52046 Phenanthrene-dl0 31.73 Hit# of 5 Tentative ID MW MolForm CAS# Qual

-Ei&SBr-"=asIA==as 188 C14D10 001517-22-2 87 2 Anthracene- 188 C14D10 001719-06-8 80 3 -Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 43 4 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . . . 188 C14H20 1000215-61-8 42 Abundance Scan 4915 (31.958 min): 10207.D (-4904) (-) m/z 188.20 100.00% 188

5000

ee 78I 94 158 M 42 52 66 , 103 118 146 I il I 198 31 60 31.80 32.00 32.20 mTT m/z 94.10 25.25% niz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #79827: Phenanthrene-d10 188

5000 31.60 31.80 32.00 32.20 80 94 m/z 158.10 16.04% 160 30 42 52 66 . 11 108118 132 146 .I,I 170179, I | > I I I | I I J I | I I rrTrr I'l J ] I I I « FrH T TTTT ■m-p-r miz-> 10 20 30 40 50 60 70 80 90 100110120130140 150160170180190200 Abundance #79826: Anthracene-d10- US

31.60 31.80 32.00 32.20 5000 14.58%

80 94 160 17 30 42 52 66 ,! 108118 132 146 i, 170179, ' I" " I “ " I" " 11"1111" TTH' i" " ■nfe-> 10 20 30 40 50 60 70 80 90 100110 120130140 150160170180190200 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one 114 'T1 FIIII 1tS 31.60 31.80 32.00 32.20 91 m/z 186.00 13.36% 105 5000 119 65 — 41 51 .1 ii , I, 146 | 11""।"‘'i""i“"I"1 ‘i■ i1" 11'■ ■■ i"■111111111"1 r"■ i■ ■"i"1'i"■'I ■"■ i1"11"11111111" iz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 31.60 31.80 32.00 32.20

10207.D SCAN020507.M Tue May 14 14:22:13 2002 Page 5

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