GCMS analysis page for sample AE11567, May 2002

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Data File : C:\MSDCHEM\1\DATA\020521\11567.D Vial: 20 Acq On : 22 May 2002 3:08 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.43 ug/1 43707 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

T Phenanthrene -d1 0 188 C14D10 001517-22-2 72 2 Anthracene-dlO- 188 C14D10 001719-06-8 64 3 - (4-Tolyl) -3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 Pent^cyclo[7.3.1.1. (4,12) . 0 (2,7) ... 188 C14H20 1000215-61-8 33 Abundance / Scan 4914 (31.952 min): 11567.D (-4904) (-) m/z 188.15 100.00% 188

5000

66 80 94I 108 132 156 ■ "i i ■ ■ < 1 । ■ 1 ■ i 1

iz-> 0- -+ 20 40 44 60 -- । "I-rT 80 100 120 140 160 180 200 220 240 260 280 292 i ■ ■ '' t 31.60 31.80 32.00 32.20 m/z 184.20 21.39% Abundance #79827: Phenanthrene-d10 188

- 5000- 31.60 31.80 32.00 32.20 80 94 m/z 189.20 18.61% 30 52 66 0- ■ ■ i ■ ' 1 1 T' Mhd , II, 198, । 132146 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #79826: Anthracene-d1 0- 188 /........................

31.60 31.80 32.00 32.20 5000 m/z 66.20 16.59%

— 80 94 0-17,30.,526644 1*t 118132146 '''T1 1*1 l ' 1 ■ i'1 ■ ‘ i ■ ■ ■ ■ i'111111111 n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one ..। mmr i r-i | I i I | | i 188 31.60 31.80 32.00 32.20 91 m/z 94.05 15.29% 105 5000 119 41 65 78-mm 146 u 11 I' 1 1 1 r'1 1 1 I1 1 ' 1 1 1 11' ■111 ■ ■ ■ ■ i'11 ■ i'' ■ ■ i ■ ■'' i nz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 31.60 31.80 32.00 32.20

11567.D SCAN020521.M Fri May 24 09:41:22 2002 Page 6

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